Source: UNIVERSITY OF CALIFORNIA, RIVERSIDE submitted to NRP
EVALUATING THE ENVIRONMENTAL IMPACTS OF ELECTRONIC CIGARETTES
Sponsoring Institution
National Institute of Food and Agriculture
Project Status
COMPLETE
Funding Source
Reporting Frequency
Annual
Accession No.
1023504
Grant No.
(N/A)
Cumulative Award Amt.
(N/A)
Proposal No.
(N/A)
Multistate No.
(N/A)
Project Start Date
Sep 17, 2020
Project End Date
Sep 30, 2024
Grant Year
(N/A)
Program Code
[(N/A)]- (N/A)
Recipient Organization
UNIVERSITY OF CALIFORNIA, RIVERSIDE
(N/A)
RIVERSIDE,CA 92521
Performing Department
Molecular, Cell and Systems Biology
Non Technical Summary
Electronic cigarettes (ECs) are a relatively new type of environmental waste. ECs are not readily degradable in the environment, and they can leak battery chemicals, heavy metals, such as nickel and chromium, and nicotine into soil and ground water. Nicotine that leaches into the soil can be taken up by crop plants and contaminate commodities. Heavy metals and battery components can present a health risk to wildlife and humans. While cigarette butt pollution has been studied for years, we know very little about EC pollution of the environment. This study will sample EC waste in various field sites in southern California, including the UCR campus, and will establish the types of ECs that are discarded, establish the condition of the batteries, the frequency and rate of their appearance over 5 years, and how much nicotine and metal they add to natural soil and/or water resources. In parallel, we will quantify metals in EC products that have been stored, hence aged, in our lab for over 10 years. We would expect to see increases in heavy metals, which would likely leach from the filament during storage. We will compute the rate of change of metals over storage time and determine if nicotine is stable or breaks down during storage. Data from the field and lab will be compared to determine if they are congruent. Our project will be one of the first to study EC waste and its potential to harm food, water and soil and may serve as the basis for implementing regulations for the safe disposable of ECs in the future.
Animal Health Component
10%
Research Effort Categories
Basic
90%
Applied
10%
Developmental
(N/A)
Classification

Knowledge Area (KA)Subject of Investigation (SOI)Field of Science (FOS)Percent
4030199115050%
1330199115050%
Goals / Objectives
This project will address electronic cigarette (EC) waste, a new environmental pollutant that has received very little prior attention.ECs, which are not biodegradable, can contribute to environmental pollution in three ways. First, all ECs have a battery, which eventually must be discarded. There is not policy or uniform regulation on discarding of EC batteries, and they end up in the environment often in landfills or public places where their decomposition will contribute battery chemicals to the soil and water. There is also a danger that EC batteries will explode , which could initiate forest fires or other types of environmental damage. Waste trucks have recently experienced explosions thought to be due to EC batteries. Secondly, the atomizing units of ECs are made of various metal parts that include nickel and chromium, and when discarded into the environment, atomizers can contribute leachates of heavy metals to ground water and soil. Third, discarded ECs contain residual e-fluid, which contains nicotine and metals/metalloids that by themselves are toxic and may also undergo reactions to form more potent toxicants that transfer directly to the environment. All EC components add to environmental pollution and could affect drinking water, agricultural water, soil, and other natural resources, such as forests.The use of ECs has grown exponentially in the last decade. They are becoming an environmental pollutant at a rapid rate and may eventually surpass tobacco cigarettes as a major source of environmental pollution. They also present a different type of pollution than tobacco cigarettes, as they contain batteries and atomizers that are not readily degradable. Strategies to deal with EC environmental pollution are needed.We propose to examine the contribution of ECs to environmental pollution with the intent of getting in front of this problem and providing scientific data that could be used to regulate the disposal of ECs.Our lab has over 10 years of experience working with ECs. We have published papers dealing with the design, evolution, topography, metal content, aerosol composition, cytotoxicity, health effects, and flavor chemicals in these products. We have also done work showing the EC aerosols deposit and remain on surfaces. We have collected EC products over the past 10 years and saved samples of both unused and used ECs, which will be analyzed in inthis project. The represents a unique collection of ECs that will enable us to determine how e-juice ages and what chemicals accumulate in aged products. For example, nickel and chromium likely leach from the filament over time and their concentrations in e-fluid would be expected to increase. Metals may also be higher in fluids from used ECs than from unused products as the filaments become delicate and the solder joints become friable with use, making accumulation of metals in fluids more likely. EC are very leaky, and their contents could readily leach into the environment. Our collection of "aged" EC is unique and will provide the first information on chemicals/metals in EC products that have aged over 10 year.Objectives: The overall objective of our Hatch project is to understand how ECs contribute to environmental pollution that could affect agriculture and directly and/or indirectly affect human health. This proposal will deal specifically with: (1) the distribution of EC waste in the environment and the condition of this waste in various locations in Southern California, including the UCR campus, and (2) the effects of aging on the composition of the e-fluids and the leaching of heavy metals from the atomizers into e-fluids using a unique collection of "aged" EC products available in our lab. Objective #1: To collect, inventory, and catalogue EC waste from various sites in southern California and to analyze metals and nicotine in the e-fluid residues in these products. This Objective will clarify the types of waste (batteries, pods, etc) and the types of ECs (disposables, Mods, cig-a-likes) that appear in the environment as waste..Objective #2: To quantify metals and nicotine in e-fluids from used and unused ECs that have been stored in laboratory-controlled conditions for various periods of time up to 10 years and to compare these data from the data collected in field sites in Objective #1.
Project Methods
Objective #1: Undergraduate students will collect, photograph, inventory and catalogue EC waste found in various field sites in southern California. This will be a longitudinal study that will track the types and amount of waste over the duration of the project. We will determine the main components, products, and brands that comprise EC waste. We will also analyze metals in residual fluids and determine the volumes of fluids in waste products. Samples will be collected on the UCR campus, around high schools and middle schools, in state parks and in other public areas. When we locate hot spots (areas where EC discards are abundant), we will continue to sample those areas over the duration of the project. We will add new hot spots as they are discovered. These data will enable us to model the level of contamination in the environment in Southern California. Specifically, we will be able to categorize the type of ECs (pod, Mod etc.) that are accumulating in the environment, the rate of accumulation, and if accumulation increases as EC use increase. We will also be able to determine which metals are likely to leach into the environment, the condition of the batteries (leaking or intact), and the amount of nicotine that could contaminate soil/water.Objective #2: Metals will be quantified in residual EC fluids using the Perkin-Elmer 7300DV inductively coupled plasma optical emission spectrometer (ICP-OES), located in Environmental Sciences. Methods for performing ICP-OES have been described previously (Williams et al 2019b). We will assay 10 metals/elements that we have previously shown to be in atomizers and e-fluids that could threaten plant and animal health. Work will begin using a collection of aged ECs that we have maintained in the lab for 10 years. The collection contains both unused and used products, and we have complete records on how much use each product received. This will provide unique information on aging of EC products in controlled laboratory conditions over a 10-year period. Objective #1 will provide metal/element data on samples collected in field sites, and the two sources of data will be compared. We will also begin to age new EC products immediately and follow their fluids over the period of the project to determine which metals accumulate in e-fluid and their rate of accumulation. This will be done by storing multiple samples of each product and removing individual samples for analysis every 6 months over 4 years. The products currently marketed are quite different than those we purchased 10 years ago and so the way in which they age may also differ. Nicotine concentrations will be quantified in samples in this Objective to determine how much nicotine would be released into soil/water when the e-fluid reservoir degrades. Location of work, facilities needed and available: The work will be performed on the UCR campus and in various field sites in southern California. Field samples will be collected on the UCR campus (even though UCR is a tobacco-free campus, numerous EC discards can be found in key hot spots) and in various other sites in Riverside and southern California locations. These include state parks, high schools, and shopping centers. When hot spots are located, they will be revisited periodically to monitor the rate of waste accumulation. Metal analyses will be done at UCR with instrumentation available in the Environmental Science Core. All other procedures will be done at UCR in the Talbot lab.Means of analysis, assessment and interpretation of data: Data in Objective #1 will be stored digitally with three backups of the original data. Data will be analyzed to determine: the type of EC contributing to waste (pod, mod etc.), the locations where waste is found, the rate at which waste accumulates, the concentrations of metals and nicotine in waste products, and the condition of the batteries. In Objective #2, ICP-OES data will be analyzed to determine the concentration of metals/elements in EC products before and during storage in the laboratory. Comparisons of means between storage times will be made using a one-way analysis of variance followed by Dunnett's posthoc test in which each time is compared to the unaged products. For both objectives, the concentrations of metal and nicotine will be compared across product type (pods, mods etc.). We would expect larger more powerful product (such mods) would produce more metal and those with larger reservoirs would be able to release more nicotine and metals. Data from the two Objectives will be cross-compared to determine how laboratory controlled data relate to data collected in field sites.

Progress 09/17/20 to 09/30/20

Outputs
Target Audience:A paper is in press that characterizes the metals in pod style electronic cigarettes (EC). When published, these data will be available to other scientists and to regulatory agencies that will have an interest tracking potential soil and water pollutants originating in EC waste. Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided?A graduate student and postdoc had the opportunity to work on this project this year. In addition, they both attended our weekly group lab meeting and our one-on-one weekly lab meeting with the PI of the project. Both the graduate student and postdoc are presenting their data at the annual meetings of the Society of Toxicology this March. They have also attended 3 virtual meetings this year to broaden their contacts and to keep updated. The postdoc was also invited to give a symposium talk at a national meeting this year. They attend a weekly seminar sponsored by the Environemntal Toxicology Graduate Program. How have the results been disseminated to communities of interest?Data from Aim #1 are currently in press and will be available soon to the scientific community and to others involved in Environmental Protection. These data could be valuable to regulators who have the authority to establish policies that could control the disposal of electronic cigarette waste. What do you plan to do during the next reporting period to accomplish the goals?This coming year we will continue to pursue aims one and two. We will go back to aim one and try to do the EC collection from various field sites if the COVID pandemic subsides and we are able to recruit undergraduate students for this part of the project. If we are not able to recruit, we will continue to analyze at the most popular and modern ECs to better document what they may be contributing to the environment. EC products change rapidly, and new products will be introduced this year that may differ from those reported in our current publication. We will also begin analyzing the samples that we have collected for aim #2 to see how the elements have accumulated in samples that have been stored over long periods of time.

Impacts
What was accomplished under these goals? Objectives: This proposal will deal specifically with: (1) the distribution of EC waste in the environment and the condition of this waste in various locations in Southern California, including the UCR campus, and (2) the effects of aging on the composition of the e-fluids and the leaching of heavy metals from the atomizers into e-fluids using a unique collection of "aged" EC products available in our lab. Impact: The unregulated disposal of electronic cigarettes (ECs) creates a new type of environmental pollution. The accumulation of this type of waste and its effect on animal and plant species is not yet understood. We do know from prior work on tobacco cigarettes that butt waste does contaminate soil and water and can threaten animal and plant health. We are characterizing the chemicals, including metals present in ECs, as a step to determining what elements and organic chemicals they can contribute to the environment. The overall objective of our Hatch project is to understand how ECs contribute to environmental pollution that could affect agriculture and directly and/or indirectly affect human health. Objective #1: To collect, inventory, and catalogue EC waste from various sites in southern California and to analyze metals and nicotine in the e-fluid residues in these products. This Objective will clarify the types of waste (batteries, pods, etc) and the types of ECs (disposables, Mods, cig-a-likes) that appear in the environment as waste. Because our campus shut down during COVID and undergraduate students were not available for this aim, we pursued this objective using a different tactic. Pods style ECs are currently the most popular and comprise a major fraction of the market. Thus, they are likely to be the most important contributors to environmental waste. We therefore purchased various types of pod-style ECs and analyzed the metals in their atomizers. Eleven EC pods from six brands/manufacturers were purchased at local shops and online. Pods were dissected and imaged using a Canon EOS Rebel SL2 camera. Elemental analysis and mapping of atomizer components was done using a scanning electron microscope coupled with an energy dispersive x-ray spectrometer. EC pods varied in size and design. The internal atomizer components were similar across brands except for variations occurring mainly in the wicks and filaments of some products. The filaments were either Elinvar (nickel, iron, and chromium) (36.4%), nichrome (36.4%), iron-chromium (18.2%), or nickel (9%). Thick wires present in 55% of the atomizers were mainly nickel and were joined to filaments by brazing. Wire-connector joints were Elinvar. Metal air tubes were made of Elinvar (50%), nickel, zinc, copper, and tin (37.5%), and nickel and copper (12.5%). Most of the wick components were silica, except for two pods (PHIX and Mico), which were mainly ceramic. Connectors contained gold-plated nickel, iron-chromium multiple alloys of nickel, zinc, gold, iron, and copper. Wick chambers were made of Elinvar. Outer casings were either nickel, copper-tin, or nickel-copper alloys. Magnets were nickel with minor iron, copper, and sulfur. Some frequently occurring elements were high in relative abundance in atomizer components. The atomizers of pods are similar to previous generations of ECs, with the introduction of ceramic wicks and magnets in the newer generations. The elements in EC atomizers may transfer into aerosols and adversely affect health. Equally important the elements in atomizers will contribute to environmental waste and may harm both animal and plant species. In summary, we characterized the design features of pod EC, then mapped 23 elements/metals in the atomizers of pods from six manufacturers. The elements/metals in atomizers are important for two reasons. First, chronic exposure could adversely affect human health. Some of the elements/metals are known to produce disease, although this has not yet been demonstrated for the toxic elements in ECs. Secondly, EC pod products are eventually discarded into the environment, contributing to chemical pollution in water and soil. Understanding the health impact of the elements/metals in EC pods and their fate when discarded will be important when establishing regulations on their use and disposal. Objective #2: To quantify metals and nicotine in e-fluids from used and unused ECs that have been stored in laboratory-controlled conditions for various periods of time up to 10 years and to compare these data from the data collected in field sites in Objective #1. Wehave catalogued and inventoried our samples for this Aim. We will begin analysis of them this coming year.

Publications

  • Type: Journal Articles Status: Accepted Year Published: 2021 Citation: Esther E. Omaiye, Monique Williams, Krassimir N. Bozhilov, and Prue Talbot (2021) Design features and elemental/metal analysis of the atomizers in pod-style electronic cigarettes. PLOS ONE, in press