Source: MICROBIO ENGINEERING, INC submitted to NRP
CULTIVATION OF MICROALGAE FOR AQUACULTURE FEED APPLICATIONS
Sponsoring Institution
National Institute of Food and Agriculture
Project Status
COMPLETE
Funding Source
Reporting Frequency
Annual
Accession No.
1023180
Grant No.
2020-33610-31983
Cumulative Award Amt.
$100,000.00
Proposal No.
2020-01005
Multistate No.
(N/A)
Project Start Date
Sep 1, 2020
Project End Date
May 31, 2021
Grant Year
2020
Program Code
[8.7]- Aquaculture
Recipient Organization
MICROBIO ENGINEERING, INC
3988 SHORT ST STE 100
SAN LUIS OBISPO,CA 934017574
Performing Department
(N/A)
Non Technical Summary
The major innovation proposed herein is to develop more productive and easily cultivated, high value, freshwater strains of microalgae for use in hatchery-nursery operations. Avoiding the need for seawater recycle and re-use will be a major advance in this business, addressing a major opportunity. A joint venture between MicroBio Engineering Inc. (MBE), a microalgae technology developer, and Reed Mariculture Inc. (RMI) the largest global supplier of algal feeds to the aquaculture industry, this project focuses on the near-term commercial applications of microalgae to supply hatchery/ nursery operations, produced at relatively small scale, one and two acres, for applications and marketing by RMI. There are considerable opportunities for process improvements and cost reductions, as well as improved quality, specifically a higher content of omega-3 fatty acids. Although essentially all work in this field has used marine diatoms, the use of freshwater species has significant advantages in their production, and potentially even in their utilization. The need for water recirculation in algae production is a challenge, in particular where seawater supply and/or discharge is a limiting factor in production and economics. For RMI, the production of freshwater strains of Thalassiosira or, possibly, the closely related Cyclotella would solve one of the major current costs and bottlenecks in their operations. In sum, this project addresses a major opportunity for improving the competitiveness of the current US microalgae aquaculture feed industry in the global marketplace and provides a pathway to larger-scale production of microalgae feeds for aquaculture.Phase I will demonstrate the cultivation and utilization of freshwater microalgae, specifically diatoms, for aquaculture feeds in hatchery and nursery operations. Freshwater diatom species, obtained from culture collections and other sources, will be tested for growth rates and productivity in laboratory batch and continuous cultures and selected strains will be cultivated in 3.5 m2 raceway ponds in a greenhouse. The objective is to obtain biomass productivity data over six months, allowing extrapolation to year-round production. Algae will be harvested by centrifugation and supplied to RMI as refrigerated concentrates, and used to feed rotifers, to demonstrate their suitability for use in aquaculture feed applications. Successful demonstration of the efficacy of using freshwater diatoms as feeds will allow a major reduction in costs by eliminating the expense of seawater supply and recirculation. Phase II will demonstrate increased production rates to further reduce costs and increase outputs. Freshwater microalgae feed production will allow RMI to retain its position as the leading supplier of microalgae feeds to the hatcheries and nurseries worldwide, protecting and expanding US jobs and exports. This project will also provide a stepping-stone towards the longer-term development of bulk microalgae feeds for aquaculture, to replace fish oil and other high-value ingredients.In brief, the specific, near-term benefits of this project are in the development of new lower cost sources of diatom aquaculture feeds for hatchery/nursery operations. RMI faces significant competitive pressures from abroad in the marketing of its microalgae products - achieving the goals of the Phase I and II projects will allow it to remain competitive, and even expand operations, with both preservation and expansion of well-paying jobs and US exports. The broader national benefits are in providing a novel approach for lower cost and greater resource potential (by not requiring seawater availability) for future, larger-scale production of bulk algae biomass for animal feed ingredients.
Animal Health Component
100%
Research Effort Categories
Basic
(N/A)
Applied
100%
Developmental
(N/A)
Classification

Knowledge Area (KA)Subject of Investigation (SOI)Field of Science (FOS)Percent
40152301060100%
Goals / Objectives
The goal of Phase I is to demonstrate the cultivation and utilization of freshwater microalgae, specifically diatoms, for aquaculture feeds in hatchery and nursery operations. The successful demonstration of the efficacy of using freshwater diatoms as feeds will allow a major reduction in costs by eliminating the expense of seawater supply and recirculation.To achieve these goals the following objectives will be addressed:The growth rate and productivity of freshwater diatom strains, particularly species of Thalassiosira, will be measured in laboratory reactors in batch and continuous cultures.Following laboratory screening, chosen strains will be cultivated in 3.5m2 raceway systems in a greenhouse with the objective of obtaining biomass productivity data over six months, which would allow extrapolation to year-round production.Biomass will be harvested and supplied to Reed Mariculture Inc. and used to feed rotifers to demonstrate suitability for use in aquaculture feed applications. Biomass compositional analysis of the algae and rotifers will be performed.Objective of Phase I and II of this project is to reduce diatom costs to below $200/kg (dry basis).
Project Methods
In Phase I, MBE will demonstrate the ability to cultivate two strains of freshwater diatoms, within the order Thalassiosirales, in small-scale (3.4 m2) raceway ponds in a greenhouse, and harvesting by (centrifugation). The concentrated algal biomass will then be used in feeding Brachionus plicatilis rotifers by RMI. Biomass composition analysis of the algae and rotifers for C20 and C22 omega-3 fatty acid content will further support the utility and value of the algal and rotifer biomass. The anticipated results for the rotifer feeding by RMI are that both the feed utilization (in terms of rotifer growth rates, yields and composition) and quality would be similar to the marine T. weissflogii and T. pseudonanna feeds currently marketed by the company.Task 1. Initial Culture Selection. Initially, freshwater diatom strains will be screened for growth potential in Bubble Columns Photobioreactors (BC-PBR). These reactors allow comparison of cultures in parallel, under set light intensity, pH, temperature and media composition. Suitable strains are those that exhibit fast growth rates (in dilute cultures), high productivities (in light-limited cultures), and a high omega-3 fatty acid content. Initial strain selection will be based on two runs for each strain, perfromed under low and high light intensities (150 and 1500 uE/m2-s), with otherwise similar conditions (pH 7.8-8.0, with 2-4 meq alkalinity and temperature at 25 oC). Strains will be selected based on maximum growth rates (log phase of growth) and maximum productivity (during the linear, light limited, growth phase). This task will require one month, which includes project initiation and initial growth experiments. Using standard methods routinely performed at MBE, biomass determinations (ash-free dry weights, OD) and biochemical content (proteins, lipids, and carbohydrates) analysis will be performed on diatom cultures.Task 2. Greenhouse Pond Operations. The second and major technical project objective of this Phase I, is the outdoor mass cultivation of selected strains in raceway ponds inside a greenhouse at the MBE field site in Paso Robles, California. To start, two strains selected with the BC-PBR (Task 1) will be tested in duplicate ponds, and replaced by other strains if they do not grow well. During Phase I, four 3.4 m2 ponds will be operated in duplicate over six months, from August 1st to January 31st, thus permitting summer, fall and winter seasonal productivities to be monitored. The process begins with production of inoculum at the MBE laboratory in 800 mL bubble columns. At density, the culture is then transferred to 15 L panels which are used to inoculate 100 liter 0.5 m2 ponds (operated at 20 cm). These ponds are then used to inoculate the 1,000 liter 3.4 m2 ponds. It takes approximately one to two weeks to build up such a culture. The cultures will be grown with one to three harvest/dilutions per week, adjusted by season and weather to maximize productivity. The concentrated algae will be refrigerated and kept at near 0 oC until used. A two-month shelf-life has been determined by RMI to be safe for use as rotifer feeds. Algae will be supplied to RMI starting within two months of project initiation and continuing through the end of the project. The main data collected by MBE will be on productivity, determined by ash free dry weight measurements and hydraulic dilutions. Samples will also be analyzed for proteins-carbohydrates and lipids.Task 3. Rotifer Feeding Trials. The final technical objective is to test the algal biomass for suitability in microalgae feeds. This work will be carried out by rotifer feeding studies under a subcontract by Reed Mariculture Inc. (RMI) using the compact Feeding System for the rotifer Brachionus plicatilis.Rotifer feed tests will be carried out using the Compact Culture System™ (CCS) production platform, developed by RMI, and using procedures routinely employed in RMI's rotifer production systems. The CCS is essentially a scaled-down version of the 1,000 L continuous-production culture systems used by RMI to produce billions of rotifers per day. The MBE freshwater algae concentrate feed trials will employ six CCS units. One control unit will be fed RMI's standard rotifer feed, and the other test units will be fed test algae concentrates. Feed will be dosed into the CCS units hourly using multi-channel timer-controlled peristaltic pumps. Rotifers will be cultured at their optimal salinity and temperature of 15 psu and 26 °C. To prevent toxicity resulting from the accumulation of ammonia excreted by the rotifers, ClorAm-X ammonia neutralizer and pH buffer will be pre-mixed with the algae concentrate in amounts based on the nitrogen content of the feeds. Ammonia tests (API Ammonia Test Kit) will be performed daily to confirm that ammonia remains below 0.5 mg/L NH3 (the toxic form of ammonia).Daily rotifer counts will be made using Sedgewick-Rafter counting slides, and rotifer densities and egg ratios (which indicate rotifer reproductive status and overall culture condition) will be recorded. Before the daily harvest, the waste trap is removed from the CCS and the accumulated waste is flushed away with a jet of clean water, and the trap is sanitized by heating to 60 °C for 1 h before re-installing in the CCS. Daily harvests will be made by removing the appropriate volume of the culture and pouring through a 40 µm mesh screen (the waste trap of the CCS ensures that negligible amounts of particulate matter contaminate rotifer samples). Rotifer samples will then be rinsed with isotonic ammonium bicarbonate solution to remove salts and stored frozen at -20 °C for subsequent analysis (biomass dry weight yield, proximate nutritional content, and fatty acid profile). The data will be analyzed for any statistical differences in feed quality, and correlated with the algae composition.

Progress 09/01/20 to 05/30/21

Outputs
Target Audience:Aquaculture community Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided? Nothing Reported How have the results been disseminated to communities of interest? Nothing Reported What do you plan to do during the next reporting period to accomplish the goals? Nothing Reported

Impacts
What was accomplished under these goals? Executive Summary Research Objective The objective of this SBIR Phase I project was to develop production technology of microalgae biomass suitable for aquaculture feeds, in the near-term objective for hatchery/nursery applications and in the longer-term as ingredients in bulk aquaculture feeds. The focus of the Phase I project was to characterize candidate diatom strains in bench-scale and pond trials. During these trials culture productivity and stability, as well as biomass quality were assessed for a variety of centric diatom species with three promising candidates emerging from the screen. Biomass from these strains was harvested and used in diet suitability studies conducted with rotifers and oysters. This project was carried out by MicroBio Engineering Inc. (MBE), with a subcontract with Reed Mariculture Inc. (RMI) and participation of California Polytechnic State University (Cal Poly). The specific technical objective for this Phase I project was 'proof of principle' demonstration of the cultivation of specific diatoms, in raceway ponds and their use as feeds in hatcheries and nurseries for filter feeders. The Phase I data was used to prepare a Phase II proposal, focused on domesticating already commercially used species and on developing a business plan for production and marketing. Phase II was not funded. Research and Findings In brief, the Phase I research demonstrated that specific strains of diatoms could be cultivated in the lab, scaled up efficiently and maintained in 3.5 m2 ponds in a greenhouse. Biochemical analysis of the biomass and feeding trials demonstrated these strains to be suitable aquaculture feeds. The three related technical objectives for Phase I included: Laboratory-scale Cultivation and Screening of Specific Diatom Strains (Completed) Cultivation of Diatoms in Raceways and Biochemical Analysis (Completed) Animal Feeding Trials (Completed) Objective 1 was met by screening 7 different strains of diatoms in laboratory bubble column array photobioreactors to assess growth and biochemical characteristics. Objective 2 was met by cultivating three promising strains in raceway ponds with the biomass harvested analyzed for biochemical content. Objective 3 was met by using the biomass harvested above for proof-of-concept feeding trials. Applications of the Research Phase I technical objectives provided the proof-of-concept that specific diatom strains can be developed for aquaculture feeds in hatchery and nursery operations. This successful demonstration of the efficacy of using specific diatoms as feeds will allow for a major reduction in the cost of cultivation. The production technology for diatom biomass developed during Phase I can be used to increase production rates and further reduce costs in a path to the future longer-term development of bulk microalgae feeds and other high-value ingredients. Results and Discussion Results of Objective 1: Laboratory-scale Cultivation of Specific Diatom Strains (completed) The development of specific diatoms for aquaculture feeds is predicated on identifying suitable strains amenable to laboratory manipulation and scale-up for cultivation in raceway systems. Several strains were obtained from culture collections and were characterized for growth and biochemical composition in the bubble column array photobioreactors. On the last day of cultivation, biomass was harvested and lipid content was measured as Fatty Acid Methyl Esters (FAMEs). Results demonstrated that all of the strains tested contained nutritionally important omega-3 fatty acids, including EPA. Results of Objective 2: Cultivation of Diatoms in Raceways and Biochemical Analysis The focus of this objective was to demonstrate scale-up and cultivation of diatoms in specific media in open raceway ponds and to generate diatom biomass for biochemical characterization and animal feeding trials. Pond cultivation was conducted over two Trials. These cultivation studies were conducted in late fall to winter in California. Starter cultures were expanded over one week to 40 L in the laboratory and then used to inoculate a single 1,000 L pond. During the first week in the greenhouse, strains were allowed to acclimate to pond conditions and then maintained semi-continuously over time. In brief, all three diatom strains tested exhibited robust and stable growth in open raceway ponds in a greenhouse during fall and winter months in California. Biomass was harvested and the biochemical profile for each strain was analyzed and determined to contain omega-3 fatty acids. Report on Results of Objective 3: Animal Feeding Trials (Completed) The goal of Objective 3 was to demonstrate the suitability of diatoms for aquaculture feeds. Proof of concept, feeding trials were conducted with rotifers and bivalves in the Phase I. Rotifer Feeding Trials Although not the target organism for the feed development proposed in Phase II, a trial was conducted with rotifers to demonstrate the suitability of specific diatoms. Cultures of the rotifer Brachionus plicatilis and six Compact Culture Systems (CCS) (https://reedmariculture.com/products/ccs?variant=39312648011881) were obtained from our project partner, Reed Mariculture, Inc. Peristaltic pumps were used for continuous feeding and sufficient equipment was available for feed trials to be conducted in triplicate. Moisture and ash content were determined for the diatom biomass harvested from raceway ponds as well as the Chlorella and yeast cake used as control feeds. Results from the feed suitability trials, based on Egg Ratio, a metric of health and fertility, indicated that the freeze dried diatoms strain #1 and strain #2 as well as Chlorella and yeast cake were sufficient to maintain health in rotifer cultures for up to 17 days. Rotifers fed a diet of diatoms had higher levels of nutritionally important omega-3 fatty acids. Oyster Clearance Trials Beyond the scope of the Phase I project, clearance trials were conducted with Pacific oysters as a proof-of-concept that specific diatoms are a suitable feed product for bivalves, the target aquaculture organisms for Phase II. Trials were conducted with the diatom product as a slurry and also as freeze-dried powder. For comparison, freeze-dried Chlorella (from RMI) and Thalapure® Mollusca (by Tomalgae) were also tested. Results demonstrated that oysters were capable of consuming specific diatom strains administered as either a slurry or a freeze-dried powder that was resuspended. These initial trials were successful in demonstrating that our diatom strains are suitable feeds for bivalves, foundational work that will be optimized and advanced in Phase II. Phase I Conclusions Phase I had three main objectives to advance the use of specific diatoms for aquaculture feeds: Objective 1 was met by screening strains of diatoms in bubble column array photobioreactors to assess their growth and biochemical characteristics. From multiple strains screened, three emerged as promising for continued study. In Objective 2 the three strains chosen in Objective 1 were successfully scaled up and cultivated in open raceway ponds. All three strains exhibited robust growth during the fall and winter seasons, demonstrating that specific diatoms can be cultivated successfully at larger scales and cooler temperatures. Biomass was readily harvested and biomass quality assessed. In Objective 3, feed trials were conducted to demonstrate their suitability for aquaculture feeds. The conclusion from the Phase I research is that production of these diatoms for aquaculture feeds is technically and economically feasible, and can be greatly improved with better adapted strains, the subject of the Phase II proposal. Phase II was not awarded.

Publications


    Progress 09/01/20 to 04/30/21

    Outputs
    Target Audience: Nothing Reported Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided? Nothing Reported How have the results been disseminated to communities of interest? Nothing Reported What do you plan to do during the next reporting period to accomplish the goals?During the next reporting period, data from the remaining pond trials will be analyzed. The animal feeding trials, including rotifers and bivalves, will be completed and the data analyzed. Results will be used to reassess the cost of freshwater diatom production for aquaculture feeds. Additional information addressed above will be provided.

    Impacts
    What was accomplished under these goals? 1. Seven freshwater and euryhaline diatom strains were obtained and screened in bench-scale photobioreactors for growth and productivity. Biomass composition was also determined. 2. Based on laboratory data, three strains were chosen for scale-up and outdoor cultivation in 1,000 L open raceway systems in a greenhouse. These strains demonstrated robust and stable growth in freshwater in raceway ponds during fall and winter seasons. 3. Diatom biomass from the three strains was harvested and proximate analysis is underway. The rotifer and bivalve feeding trials are currently being performed by MicroBio Engineering with equipment supplied by Reed Mariculture. 4. Data analysis is underway.Results will be used to reassess the cost of freshwater diatom production for aquaculture feeds.

    Publications