Source: UNIV OF WISCONSIN submitted to NRP
REGULATION OF HEPATIC AMINO ACID EXTRACTION IN LACTATING DAIRY COWS
Sponsoring Institution
National Institute of Food and Agriculture
Project Status
COMPLETE
Funding Source
Reporting Frequency
Annual
Accession No.
1020476
Grant No.
(N/A)
Cumulative Award Amt.
(N/A)
Proposal No.
(N/A)
Multistate No.
(N/A)
Project Start Date
Oct 1, 2019
Project End Date
Sep 30, 2023
Grant Year
(N/A)
Program Code
[(N/A)]- (N/A)
Recipient Organization
UNIV OF WISCONSIN
21 N PARK ST STE 6401
MADISON,WI 53715-1218
Performing Department
Dairy Science
Non Technical Summary
Nitrogen is an expensive nutrient and environmentally harmful waste product. Under current nutritional practices, 75% of the nitrogen consumed by a lactating dairy cow is excreted in manure. To feed the growing world population, while maintaining fresh water and air quality, dairy systems need to drastically increase nitrogen efficiency. Our long-term goal is to develop dietary strategies that increase productivity of dietary protein and reduce N excretion in manure.The majority of nitrogen losses occur in the liver when amino acids (AA) are converted to urea. The overall hypothesis is that stimulation of hepatic anabolic activity increases splanchnic extraction of AA but reduces urea production. Using dietary approaches and a splanchnic multi-catheterized dairy cow model we aim to:Determine the effect of amino acid supplementation on splanchnic AA extraction and metabolism.Analyze the effect of dietary energy sources on splanchnic AA fluxes.Investigate cellular mechanisms of insulin and AA regulation of hepatic metabolism.Update a lactating dairy cow model of hepatic AA metabolism.This project contributes to more efficient milk production, reduced environmental impact of U.S. dairy systems, and satisfaction of humanity's need for high-quality food. Our overall research program on liver and mammary metabolism could lead to an increase in nitrogen efficiency of 50% (to 37.5% nitrogen efficiency), which considering the 9.4 million dairy cows in the U.S., would translate into more than one million acres of protein production land released and 100 tons less nitrogen excreted in dairy cattle manure yearly.
Animal Health Component
40%
Research Effort Categories
Basic
60%
Applied
40%
Developmental
0%
Classification

Knowledge Area (KA)Subject of Investigation (SOI)Field of Science (FOS)Percent
30234501010100%
Knowledge Area
302 - Nutrient Utilization in Animals;

Subject Of Investigation
3450 - Milk;

Field Of Science
1010 - Nutrition and metabolism;
Goals / Objectives
The long-term goal of this proposal is to identify dietary strategies that maximize AA utilization for milk protein synthesis and minimize splanchnic AA catabolism and N excretion. Within this proposal, we aim to understand AA and energy regulation of pDVC and hepatic AA extraction and metabolism. We hypothesize that mTORC1 mediate effects on splanchnic extraction of AA increase reversible splanchnic use of N (e.g. protein synthesis) and reduce irreversible N conversion to urea for excretion.The specific objectives are:Determine the effect of G1AA and BCAA on splanchnic individual AA fluxes, hepatic metabolism and urea output, and milk components yield in dairy cows.Analyze the effect of dietary energy sources on BCAA regulation of splanchnic individual AA fluxes, hepatic metabolism, and milk components yield in dairy cows.Determine the role of insulin on G1AA and BCAA stimulation of hepatic mTORC1 activity in lactating dairy cows.Incorporate nutritional regulatory mechanisms into a mathematical model of hepatic AA metabolism in the lactating dairy cow.
Project Methods
Objective 1:Treatments will consist of abomasal infusion of water (negative control), His and Met (1:1 mass ratio) or the BCAAs Ile and Leu (0.6:1 mass ratio) to reduce the MP deficiency by 50% (12.5% deficiency), or the combination of both EAA groups to meet MP requirements. Ruminally cannulated multiparous cows will be fixed with indwelling catheters in a jejunal branch of the mesenteric artery, a duodenal branch of the mesenteric vein, a small branch of the right ruminal vein, portal vein, and a small branch of the hepatic vein, at least 4 weeks before the beginning of the experiment as previously described (Huntington et al., 1989).Cows will adapt to the experimental diet for 2 weeks before starting infusion. Infusion periods will be 10 days long with 6 days wash out period in between. Diets will be restricted to 95% of the intake during the adaptation period. During AA infusion, diets will be fed in 6 equal meals and every 2 hr for the last 24 hr. Feed consumption will be recorded at every meal. Milk production will be measured in every milking from infusion day 6 to 10, and milk composition will be analyzed in composed samples from those 8 milkings. Body weight will be recorded at the beginning and end of each period for two consecutive days.On the last day of AA infusion pAH will be continuously infused into the mesenteric and ruminal vein for 4 hr at a rate of 6 g/h (12 g/h total) to determine blood flow (Larsen et al., 2015), and arterial, portal and hepatic vein samples will be collected every 30 min. Hematocrit will be determined immediately after sampling in arterial samples by centrifugation in capillary tubes at room temperature (20ºC). Blood samples will be immediately cooled on ice. Glucose, lactate, BHBA, urea-N and ammonia-N will be analyzed from deproteinized whole blood samples. Plasma will be isolated by centrifugation and pAH, individual AA, VFA, NEFA, triglyceride, insulin, albumin and total protein will be analyzed. For AA analysis, plasma samples will be gravimetrically combined with13C universally labeled internal AA standards for LC-MS analysis.Objective 2:Peak lactation dairy cows will be fed isoenergetic high starch or high fiber diets to meet NEL requirements, with adequate levels of RDP and limited RUP to generate a 25% MP deficiency (NRC, 2001). Under each dietary treatment, water or the BCAAs Ile and Leu (0.6:1 mass ratio) will be abomasally infused to reduce the MP deficiency by 2 thirds. The effect of BCAA infusion on visceral and hepatic individual AA clearance rate constants will be compared under the two dietary energy sources in a 2 by 2 factorial arrangement of treatments.Ruminally cannulated multiparous cows will be fixed with indwelling catheters as described above. Infusion periods will be 10 days long plus 6 days for diet adaptation or infusion wash out, and 10 days for infusion of each group of EAA. Diets will be restricted to 95% of the intake during the adaptation period for the lowest intake treatment. During AA infusion, diets will be fed in 6 equal meals and every 2 hr for the last 24 hr. Feed consumption will be recorded at every meal. Milk production will be measured in every milking from infusion day 7 to 10, and milk composition will be analyzed in composed samples from those 8 milkings. Body weight will be recorded at the beginning and end of each period for two consecutive days.Infusions and sample collection and analysis will be as described in Objective 1. Dietary energy source and EAA infusion effects and interactions on dependent variables will be analyzed with a mixed model in R, with random effects of cow and period and fixed effects of energy, BCAA and the interaction within cow and period. Repeated measures within infusion periods will be considered for not composed samples.Objective 3:An independent study to this proposal will be performed to determine the effect of insulin on G1AA and BCAA stimulation of mammary AA extraction and milk protein synthesis in lactating dairy cows. Either water, the G1AA His and Met, or the BCAA Ile and Leu will be infused for 10 days. On day 7 of AA infusion, cows will be subjected to insulinemic-euglycemic clamp, where insulin will be continuously infused to rise plasma insulin concentration, and glucose will be infused at the required rate to maintain euglycemia. Liver biopsies will be collected on day 6 (pre-clamp) and day 10 (clamped) of abomasal infusions to determine the effect of insulin on G1AA and BCAA stimulation of mTORC1 signaling, mRNA expression of metabolic enzymes, and tissue free AA concentrations.Liver tissue samples will be flush frozen in liquid N and stored at -80ºC for analysis. Frozen tissue will be lysed with 1.0 mm glass beads in a Mini-Beadbeater-24. For LC-MS analysis of tissue lysates will be deproteinized in perchloric acid, filtered (0.2 μm) and 2 μL will be injected into a quadrupole LC-MS for analysis. Standard curves will be generated for each AA. For qPCR analysis of mRNA expression, tissues will be homogenized in TRI Reagent (Sigma) and RNA will be extracted following provider instructions. Complementary DNA (cDNA) will be synthesized from RNA (1μg) by Superscript III reverse transcriptase (Invitrogen) in a thermocycler. Primers for target genes including in the mTORC1 pathway (AKT1, TSC1, TSC2, MTOR, RPS6KB1, EIF4BP1), ribosomal RNA genes (18S and 28S), and AA transporters (SLC1A1, 1A5, 3A2, 7A1, 7A5, and 36A1) will be designed with the IDT primer design tool, and real time PCR will be performed using SYBR Green dye-based PCR amplification in a BioRad Real Time PCR machine. Protein expression and phosphorylation of proteins in the mTOR pathway including Akt, mTOR, S6K, 4E-BP1 and rpS6 will be determined by western blotting as previously described (Arriola Apelo et al., 2014b).Objective 4: The current hepatic model (Hanigan et al., 2004a) will be evaluated by residual analysis with literature and experimental data. If as expected, model reparameterization is required, up to three possible mathematical functions will be considered based on error pattern (e.g. linear, quadratic, and exponential). Revised model parameterization will be performed by the maximum likelihood method using the Nelder-Mead algorithm (Press, 2007). Prediction errors will be randomly sampled to generate a population of parameter estimates by non-parametric bootstraping (Efron and Tibshirani, 1993). Means, standard errors, and 95% confidence intervals of that population of parameters will be used as descriptors of model parameters. A multivariate analysis based on AIC and residual analysis will be performed using mean parameter values to compare the original and revised model. Global sensitivity analysis of the final model will be performed for input variable and individual function parameters (Saltelli et al., 1999).

Progress 10/01/19 to 09/30/20

Outputs
Target Audience:We presented two abstracts in the American Dairy Science Association Annual Meeting, which is attended by scientists and field technical support for dairy producers (e.g. dairy nutritionists). Changes/Problems:We were not able to perform multicatheterization because the university banned visits to campus due to the Covid-19 pandemic, and we needed the assistance of Dr David Harmon from University of Kentucky for this trial. To partially overcome that limitation, we did two trials with different experimental approaches that allow us to see the effect of AA by themselves and in combination with insulin. In the first trial, we performed liver biopsies so we studied liver metabolism, although not fluxes. The proposed surgical procedure and study are still planned for 2021 or 2022, depending on the limitations that we encounter due to the pandemic. What opportunities for training and professional development has the project provided?Undergraduate and graduate students were trained in different animal and laboratory techniques. The graduate student on the project received training in catheterization, biopsies, surgical procedures, intra-venous infusion, and molecular biology techniques including, western blotting, ELISA, and mass spectrometry. Undergraduate students with a major in biochemistry and no cow experience, received training in cow handling, tail and mammary vein blood sampling and health evaluation (temperature and respiration rate). They also received training in molecular biology techniques. One of the undergraduate students has developed an expertise in mass spectrometry. Other students have been trained in sterile techniques, and tissue lysing. How have the results been disseminated to communities of interest?Preliminary results of the studies have been presented at the American Dairy Science Association Annual Meeting where scientists and nutritionists can benefit from our findings. They have been presented in seminars on campus, including the Department of Animal and Dairy Science Graduate Seminar and Endocrinology and Reproductive Physiology seminar. What do you plan to do during the next reporting period to accomplish the goals?We plan to analyze plasma and biopsy samples from the completed studies, perform a cow trial, present further results at scientific meetings, and publish our findings.

Impacts
What was accomplished under these goals? Objective 1: In one of the abstracts presented at ADSA annual meeting, we reported the effect of BCAA, Met, His and Lys on milk components yield and urea output. Amino acids did not have the hypothesized effect on milk protein production. However, to our surprise we saw a significant effect of mTOR-stimulating amino acids in milk and de novo milk fat synthesis. In that study, we also collected liver biopsies that we will use to understand the effect of those amino acids in hepatic metabolism. Objective 2: We used two different energy sources, lipogenic and glucogenic, to determine if the effect of amino acids was conditional to the energy source. We observed a significant effect of energy source, in which mTOR-stimulating amino acids stimulated de novo milk fat synthesis only under glucogenic energy supplementation. We collected liver biopsy samples to determine ifenergy source conditions the effect of amino acids on liver metabolism. That work will be accomplished in 2021. Objective 3: We performed an hyperinsulinemic-euglacemic clamp to determine ifinsulin conditions the effect of amino acids. The production part of that study was presented this year at ADSA annual meeting. We are analyzing blood samples to complete the manuscript in 2021. Objective 4: not addressed yet.

Publications

  • Type: Journal Articles Status: Published Year Published: 2020 Citation: Pszczolkowski VL (G), Arriola Apelo SI. The market for amino acids: understanding supply and demand of substrate for more efficient milk protein synthesis. Journal of Animal Sci Biotechnol. 2020. 11(1):108. doi: 10.1186/s40104-020-00514-6. Invited Review.
  • Type: Journal Articles Status: Published Year Published: 2020 Citation: Pszczolkowski VL, Zhang J, Pignato KA, Meyer EJ, Kurth MM, Lin A, Arriola Apelo SI. Insulin potentiates essential amino acids effects on mechanistic target of rapamycin complex 1 signaling in MAC-T cells. Journal of Dairy Sci. 2020. 103(12):11988-12002. doi: 10.3168/jds.2020-18920.
  • Type: Journal Articles Status: Published Year Published: 2020 Citation: Pszczolkowski VL, Halderson SJ, Meyer EJ, Lin A, Arriola Apelo SI. Pharmacologic inhibition of mTORC1 mimics dietary protein restriction in a mouse model of lactation. Journal of Animal Sci Biotechnol 2020. 29(11):67. doi: 10.1186/s40104-020-00470-1.