Source: UNIVERSITY OF MAINE submitted to NRP
INTEGRATED OPTIMIZATION OF MICROBIAL, CHEMICAL, AND SENSORY ASPECTS OF NON-DAIRY, LOW-ALCOHOL FERMENTED BEVERAGES: KOMBUCHA AND WATER KEFIR
Sponsoring Institution
National Institute of Food and Agriculture
Project Status
COMPLETE
Funding Source
Reporting Frequency
Annual
Accession No.
1018506
Grant No.
2019-67018-29189
Cumulative Award Amt.
$193,566.00
Proposal No.
2018-06582
Multistate No.
(N/A)
Project Start Date
Sep 1, 2019
Project End Date
Aug 31, 2023
Grant Year
2019
Program Code
[A1361]- Improving Food Quality
Recipient Organization
UNIVERSITY OF MAINE
(N/A)
ORONO,ME 04469
Performing Department
(N/A)
Non Technical Summary
Consumer interest in fermented foods is steadily increasing in the United States. A subset of these products is beverages produced with the use of yeast and bacteria together in a symbiotic mass (SCOBY). The microorganisms in SCOBY systems are very diverse and variable, which causes the products to look, smell and taste different. In addition, presence and amount of health promoting compouds may vary significantly from product to product. This project will look at the natural variation in culture composition, the factors that influence composition and their effects on finished product, with the goal of helping the industry to standardize products in order to maximize health benefits and consumer acceptability.
Animal Health Component
100%
Research Effort Categories
Basic
(N/A)
Applied
100%
Developmental
(N/A)
Classification

Knowledge Area (KA)Subject of Investigation (SOI)Field of Science (FOS)Percent
7015010104050%
7015010309030%
7015010100020%
Goals / Objectives
This project aims to improve knowledge of various aspects of non-dairy, low alcohol fermented beverages. Using a next-generation sequencing approach to assess culture systems and beverages, we will generate more reliable, complete data regarding the composition of the products, giving insight into methods for targeting a defined finished product. Commercial, dried versions of cultures for these products are not currently available from any source. Consistency of product suffers as a result, resulting in a high potential for alienation of consumers. As part of this project, we will generate valuable information about consumers of fermented beverages, their expectations with regard to sensory and health beneficial characteristics of such products. This combination of comprehensive microbiological, biochemical, and consumer data will generate approaches for optimizing product quality and market potential.
Project Methods
Fermented beverages will be produced in non-sterile ½ gallon glass jars. Kombucha and water kefir fermentations will be monitored daily until pH reaches 3.0 and 4.0 respectively, at which point samples of culture biomass and fermentate will be taken aseptically. DNA will be extracted using the MoBio PowerFood Microbial DNA Isolation Kit. DNA extracts will be frozen at -80C until being sent for sequencing. Whole-sample DNA extracts will be used as templates for amplification of the D1-D2 region of the eukaryotic large subunit (LSU) rRNA gene, and V1-V3 region of the prokaryotic 16S rRNA gene, enabling profiling of yeast, mold and bacterial populations based on relative proportions of discrete ribotypes, following previously published protocols. Indexed and pooled amplicon libraries will be subjected to high throughput DNA sequencing on the Illumina MiSeq platform. Analysis of these datasets will give more in-depth information regarding the effects of heterogeneity among the microbial profile of SCOBYs and resulting products, and the reproducibility of kefir and kombucha produced by a given SCOBY over multiple passes or generations.Simultaneously, cultures will be grown as described to produce sufficient biomass for preservation by ultralow temperature freezing (-80°C) and lyophilization. In a subsequent set of experiments, preserved cultures will be compared side-by-side to fermentations started with "daughter cultures" collected from repeated generation cycles (generations 10 and 20 from original cultures). Fermentation efficacy and duration (to previously identified pH targets) will be monitored, and samples of finished products will be collected to compare microbial composition as previously described. These experiments will assess the feasibility of starter culture preservation and degree of community temporal drift in traditionally propagated culture systems.From the culture systems analyzed, a maximum of three from each product category will be used to investigate the effects of fermentation time and refrigerated storage on the resulting product. Extended fermentations of up to 6 days for water kefir and 30 days for kombucha will be conducted utilizing conditions previously described. Fermentate will be analyzed intermittently at predetermined sampling points for simple sugars (fructose, glucose, sucrose), organic acids (lactic, acetic and gluconic) and ethanol concentrations. pH will be measured at each sampling time. A subset of samples from duplicate fermentations will be pooled and subjected to metagenomic sequencing as previously described. These data will provide a picture of metabolite production during the course of beverage fermentation. By combining analytical data with sequencing results, the relationship between microbial community structure and finished product characteristics can be elucidated. A subset of treatments (2, 4 and 6 day water kefir fermentations and 10, 20 and 30 day kombucha fermentations) will be replicated for shelf life analysis. At the conclusion of fermentation, fermentate will be aseptically separated into sterile conical tubes and refrigerated for up to 90 days. At two week increments, samples will be analyzed by HPLC/RID as described, spectroscopy to determine turbidity and cultural enumeration of fungi, total aerobic mesophiles, and lactic acid bacteria, using established methods (29). The visual presence of culture biomass and pH will also be recorded. These data will provide insight into the stability of unpasteurized fermented beverages during storage, as well as changes to visual attributes over time.Permission to conduct research with human subjects will be obtained from the University of Maine Institutional Review Board. An internet survey of 2000 U.S. adults at least 18 years old will be conducted. Qualtrics software (Provo, UT) will be used to create and administer the survey. Survey participants will be screened for consumption of water kefir and kombucha during the previous 18 months. The survey instrument will collect demographic data and contain questions designed to quantify low-alcohol fermented beverage purchase and consumption habits and to identify major barriers to consumer acceptance of these products. Photographs of beverages with different colors, clarity, and presence of clumps and sediment will be presented to classify visual preferences of specific consumer demographic groups. For example, do some consumers like cloudy drinks with sediment because they believe the traits indicate less-processing or more health benefits?A minimum of 100 adult consumers from greater Bangor, ME will be recruited to participate in each of two acceptability tests for water kefir and kombucha, respectively. The UM Sensory Evaluation Center has 12 Hewlett Packard ElitePro tablets available to collect data. The Center has 12 partitioned cubicles constructed with controlled Daylight 65 lighting and temperature and airflow control. Questionnaires, experimental designs, and statistical analyses will be created with SIMS sensory evaluation software (v. 6.0, Sensory Computer Systems, Berkeley Heights, NJ). The standard 9-point hedonic scale (1= dislike extremely; 5 = neither like nor dislike; 9= like extremely) will be used to assess liking of appearance, color, aroma, body (viscosity), flavor, degree of carbonation, and overall acceptability of samples. Just-about-right (JAR) scales will be used to assess consumer opinions of cloudiness/clarity, sweetness, tartness/acidity, and viscosity. Demographic questions including age, gender, kombucha (or water kefir) purchase habits, and purchase intent will also be asked. No more than five samples will be served in a single test to avoid sensory fatigue; samples will be served at 5°C. In year 2 , formulations based on the overall liking and JAR results for each product category will be tested with 100 interested consumers to confirm the suitability of the formulations. The unique approach to relating chemical constituents to consumer liking can provide a framework for quality assurance recommendation for fermented drink processors.The biochemical content of these fermented beverages will be identified and quantified using high performance liquid chromatography (HPLC) and will focus on the major flavor components - acids (acetic, lactic and gluconic) and residual sugars (fructose, glucose and sucrose). Ethanol, methanol and other minor organic acids will be monitored by HPLC, as well. Turbidity will be measured with a Hanna HI847492 haze turbidity meter for beer (Woonsocket, RI); CIE L*a*b* color will be measured with a Hunter Labscan colorimeter.

Progress 09/01/19 to 08/31/23

Outputs
Target Audience:The target audiences for this project comprise academic researchers and industry members. Academic researchers were targeted mainly through conference presentations and posters as well as peer reviewed publications (forthcoming). Industry members were targeted during the performance period through presentations at trade shows and will continue to be targeted by publication of extension materials. Changes/Problems:The only significant challenge encountered was the inability to work with human subjects during the period of the pandemic. Unfortunately, this prevented the completion of planned human sensory tests, additional emphasis was placed on survey work as a result. What opportunities for training and professional development has the project provided?Across the duration of this project, two undergraduate, three graduate and one post-doctoral student have been trained. Training has included one-on-one work with faculty or senior student mentors. These students have also enjoyed professional development activities in the form of preparation and presentation of research findings at academic meetings and conferences including local and national scales. How have the results been disseminated to communities of interest?At present results have been disseminated primarily through oral and poster presentations. Formal publications are in preparation. What do you plan to do during the next reporting period to accomplish the goals? Nothing Reported

Impacts
What was accomplished under these goals? The primary goals of this project included: 1. elucidation of the effect of uninterrupted culture re-use in the production of low alcohol fermented beverages and the extended evvects of culture composition on the composition of the resulting beverage during storage; 2. comparison of the microbial and chemical profiles of kombucha and water kefir; and 3. assessment of consumer awareness and preferences for kombucha beverages. Microbial cultures were brewed without interruption for 10-20 generations, including replication. During this work, both microbial counts and next generation sequencing data were collected. Cultural data were used to better understand trends in the general types and levels of organisms present in cultures in relation to beverages, and how that changed as cultures were used repeatedly. We ascertained that relative to kombucha, water kefir represents a microbial consortium that is more stable across generations, but that the integrity of the culture itself (phyically measured using turbidity and biomass accumulation) was significantly better for kombucha. These findings represent achange in knowledgethat benefits industrial producers. High throughput sequencing data were obtained for both kombucha and water kefir cultures and beverages. These data reveal significantly greater diversity within the culture system than the resulting beverages, suggesting that the surviving microbiota in fermented beverages represents a subset of cultures which have adapted to the niche of the beverage matrix. It is unknown the extent to which the bioactive consitituents (ass opposed to the live microbes) varies in the beverages due to diversity in the culture.hese findings represent achange in knowledgethat benefits industrial producers. A large scale consumer survey comprising 2,149 participants was conducted during this project. Participants were asked about their awareness, consumption of and preferences for kombucha and other related beverages. The work described here represents the largest survey on this subject to date. Kombucha consumers were likely to be young, highly educated and belonging to minority racial and ethnic identifying groups. The most frequently cited motivation for kombucha consumption was "health benefits," which was chosen over twice as freqently as either "probiotic content" or "nutrient content." The rhese findings represent achange in knowledgethat benefits industrial producers, allowing them to better target their core and/or nascent consumer bases.

Publications

  • Type: Conference Papers and Presentations Status: Published Year Published: 2021 Citation: Dankwa, A, LB Perkins and JJ Perry. Assessing the microbial variability and chemical composition in kombucha during repeated brewing cycles and refrigerated storage. Poster, International Association of Food Protection Annual Meeting, Phoenix, AZ/Virtual.
  • Type: Conference Papers and Presentations Status: Published Year Published: 2021 Citation: 1Dankwa, A, LB Perkins and JJ Perry. 2021. Assessment of microbial variation and chemical composition in water kefir over repeated brewing cycles and refrigerated storage. Oral presentation, American Society for Nutrition, Nutrition 2021, Virtual.
  • Type: Conference Papers and Presentations Status: Published Year Published: 2022 Citation: Dankwa, A and JJ Perry. 2022. Assessment of preservation techniques for kombucha starter culture. Poster, Institute of Food Technologists, IFT FIRST, Chicago, IL.
  • Type: Conference Papers and Presentations Status: Published Year Published: 2022 Citation: Camire, ME, MP Walker and JJ Perry. 2022. Characterization of U.S. kombucha drinkers. Poster, Institute of Food Technologists, IFT FIRST, Chicago, IL.
  • Type: Theses/Dissertations Status: Published Year Published: 2021 Citation: Walker, M. Consumer characteristics, acceptance and knowledge of, and preferences for kombucha. Thesis. University of Maine.
  • Type: Theses/Dissertations Status: Published Year Published: 2022 Citation: Integrated optimization of microbial and chemical composition of non-dairy, low-alcohol fermented beverages: kombucha and water kefir. Dissertation. University of Maine
  • Type: Conference Papers and Presentations Status: Published Year Published: 2022 Citation: Bromley, A and JJ Perry. 2022. Survival of probiotic Lactobacillus spp. during kombucha fermentation. Poster, International Association for Food Protection Annual Meeting, Pittsburgh, PA.


Progress 09/01/21 to 08/31/22

Outputs
Target Audience:The target audience reached during this period is limited to academic researchers. Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided?During this period twograduate (MS) students successfully defended their work and received their degrees. How have the results been disseminated to communities of interest? Nothing Reported What do you plan to do during the next reporting period to accomplish the goals?During the next reporting period, the remainder of data collection and analysis will be completed and used for the production of the dissertation of the one remaining graduate student being trained on this project.

Impacts
What was accomplished under these goals? During this reporting period, previously gathered DNA was sequenced and analysis began. Laboratory work primarily comprised assessment of the success of various preservation techniques on the survival and level of microorganisms in physical culture matrices. Experiments included the physical manipulation of cultures, use of cryoprotectants and modification of preservation modality and conditions. Additionally, the results of a previously completed consumer survey were analyzed and included in the thesis of a graduating MS student.

Publications


    Progress 09/01/20 to 08/31/21

    Outputs
    Target Audience: Nothing Reported Changes/Problems:Major problems include significant delays due to pandemic-related closures and the inability to conduct consumer sensory evaluation under pandemic operating protocols. Both of these issues have added to the expected duration of the project, but are expected to be overcome during the extension period. What opportunities for training and professional development has the project provided?The project has provided training opportunities for three graduate students, twoMS and one PhD. Both MS students are expected to graduate December 2021, one having worked on the consumer/social science aspect of the project and one having worked on the cultural microbiology/safety side of the project. The PhD student is conducting the bulk of the research, including genomics, and is expected to graduate August, 2022. How have the results been disseminated to communities of interest? Nothing Reported What do you plan to do during the next reporting period to accomplish the goals?During the next reporting period, the analysis of high throughput sequencing data will be completed. Culture preservation trials, currently underway, will also be completed. Results from the consumer survey will be used to design a consumer sensory test aimed at targeting test formulation to stated consumer preferences.

    Impacts
    What was accomplished under these goals? Significant progress has been made on several goals during this reporting period. Work on Objective 2; defining the relationship between culture composition, fermentation duration and biochemical composition of beverages, has concluded and is in the data analysis process. Likewise, the majority of work for Objective 1, which assesses diversity and temporal stability of SCOBY cultures using high throughput sequencing, has been accomplished, including metagenomic sequencing. Genomic data is currently being analyzed. Additionally, a large- scale consumer survey assessing purchase drivers and product preferences (Specific aim 3.1) was completed during this reporting period.

    Publications


      Progress 09/01/19 to 08/31/20

      Outputs
      Target Audience: Nothing Reported Changes/Problems:To date there have been no major changes to the approach planned for this project. The project team has, however, encountered delays in the execution of planned work due to unforseen facility closures related to the coronavirus pandemic. This has resulted in progress impedence, and may necessitate a time extension for project completion, but neither previous closures nor future interruptions due to additional closures are expected to result in a restructuring of original project design or execution. What opportunities for training and professional development has the project provided?To date the project has provided training opportunities for three graduate students, two at the MS level and one at the PhD level. These students have received training in literature review and experimental design within the context of the project, focusing on both microbiological and social sciences. How have the results been disseminated to communities of interest? Nothing Reported What do you plan to do during the next reporting period to accomplish the goals?The next reporting period will comprise the majority of data gathering and analysis for the project. Previously isolated metagenomic DNA will be sequenced and analyzed in order to elucidate the effects of culture system and generation on variability of microbiota in low alcohol fermented beverage products and corresponding beverages will be subjected to biochemical analyses. A previously developed consumer survey will be administered to > 1000 participants nationally to assess consumer awareness of and interest in fermented beverages. Initial work on preservation techniques for artisanal cultures will also commence during the next reporting period. Likewise, it is expected that data gathered during surveying and biochemical analyses will be leveraged in order to conduct consumer sensory testing with the goal to validate stated consumer preferences for fermented beverages (assuming no complications for in-person testing due to ongoing pandemic).

      Impacts
      What was accomplished under these goals? Sequential replication of > 10 culture systems through 20 generations was accomplished during this reporting period. Metagenomic DNA from representative generations has been isolated and preserved for use in next-generation sequencing, which will begin during Q1 of the next reporting period. Cultural enumeration of representative microbial populations has been conducted concurrently with DNA isolation for the past year in order to compare with sequencing results for contextualization of the biases inherent in both methods. Development of a consumer survey is underway with the cooperation of the trade organization Kombucha Brewers International. Survey will be conducted during the next reporting period.

      Publications