Source: TENNESSEE STATE UNIVERSITY submitted to NRP
MICROENCAPSULATION FOR TARGET DELIVERY OF ANTIBIOTIC ALTERNATIVES TO ENHANCE POULTRY PERFORMANCE
Sponsoring Institution
National Institute of Food and Agriculture
Project Status
COMPLETE
Funding Source
Reporting Frequency
Annual
Accession No.
1018068
Grant No.
2019-38821-29055
Cumulative Award Amt.
$300,000.00
Proposal No.
2018-04971
Multistate No.
(N/A)
Project Start Date
Feb 15, 2019
Project End Date
Feb 14, 2023
Grant Year
2019
Program Code
[EQ]- Research Project
Recipient Organization
TENNESSEE STATE UNIVERSITY
3500 JOHN A. MERRITT BLVD
NASHVILLE,TN 37209
Performing Department
(N/A)
Non Technical Summary
Antibiotic resistance is becoming a major health issue in the United States. Countries in the worldare striving for ways to eliminate the misuse of antibiotics in feed as growth promoters and illnessprevention intervene in livestock production. Essential oils and polyphenols are natural compoundsthat can be used as antibiotic alternatives, but their use is limited due to their sensitivity to heat andlight, and harsh flavor and taste. Microencapsulation is a promising approach to protect thesecomponents and to deliver them to the target site in the intestinal tract. This proposal fillsknowledge gaps critical to the development of antibiotic alternatives that will enhance food safety,improve poultry performance through modified intestinal microflora, and eliminate antibioticabuse. The project is designed in a series of logical, sequential objectives supported by an industrialcollaborator. The specific objectives are: 1). Optimize microencapsulation formula and methods byusing novel ingredients as wall materials; 2). Investigate the delivery efficiency and releasingprofile using in vitro and in vivo methods; 3). Evaluate poultry intestinal microflora and growthperformance after feeding micro particles through diet. This project fits into the institutional planand confronts a local and national priority, conceiving, designing and evaluating new bioprocessingtechniques in Food Safety. This project addresses the CBG Program Priority Areas, USDAPriorities and NIFA Challenge Areas in Food Safety. Outcomes yielded from the grant willstrengthen the research and teaching capacity in 1890 universities.
Animal Health Component
50%
Research Effort Categories
Basic
(N/A)
Applied
50%
Developmental
50%
Classification

Knowledge Area (KA)Subject of Investigation (SOI)Field of Science (FOS)Percent
71250102000100%
Goals / Objectives
Each year in the United States, at least 2 million people become infected with bacteria that are resistant to antibiotics, and at least 23,000 people die each year as a direct result of these infections (Center for Disease Control and Prevention, 2018). The widespread use of antibiotics on both animals and humans has contributed to the microbial resistance to antibiotics. Since January 2017, the FDA has restricted the use of some antibiotics as growth promoters, a practice that leads to antibiotic-resistant bacteria that pose threats to human health (FDA 2018). In awareness of this crisis, the consumers and markets are demanding antibiotic-free products. The world's biggest burger chain, McDonald's, announced that they will implement a new program of only sourcing chickens raised without antibiotics that are important to human medicine (USA Today, March 4, 2015). KFC announced in April 2017 that it will rid its chicken of antibioticsby the end of 2018. Tyson Foods announced that it will go antibiotic free chicken as well (USA Today, May 2, 2017). As a result, alternatives to antibiotics are in urgent need to improve digestive health and growth performance of livestock.Many natural compounds are proven with antibiotic activities and can be used as alternatives to antibiotics. In combination of encapsulation technology, these natural compounds could be delivered at target location in digestive tract, thus improving the gut health and growth performance of livestock. Therefore, this project will develop an antibiotic alternative to sustain poultry production. This project will enhance the research capacity of 1890 institutions with novel ideas and research capacity to resolve emerging issues, and will equip our underrepresented students with advanced research skills and knowledge to become highly competitive in the fast growing technology market. The proposal has obtained support from international food industry, Archer Daniel Midland (ADM), for providing research materials, and technical support regarding new ingredients in feed industry. This Food Safety research is among the top priorities in the College of Agriculture at Tennessee State University (TSU) (Letter of Support from College Dean). Recently, the Food Sciences Laboratory at TSU has received support from the college, and has acquired a number of cutting edge instruments. This project will bring together multidisciplinary expertise to enhance the collaboration among industrial stakeholders and universities.In this proposal, five major goals will be achieved: 1. Develop an antibiotic alternative product by microencapsulating essential oil and polyphenol mixtures; 2. Evaluate the delivery efficiency, releasing profile and antimicrobial effects by in vivo methods; 3. Explore a novel application of a natural ingredient in encapsulation filed; 4. Promote the application of antibiotic alternatives in poultry production; 5. Build the research capacity in Food and Animal Science Degree program at TSU by collaborating with scientists from nationally and internationally recognized institutions and industrial stakeholders.Specific Objectives are:1) Formulate and optimize microencapsulation for antibiotic alternatives; 2) Investigate the delivery efficiency, releasing profile and effects on bacteria of the microparticle using in vitro methods; 3) Evaluate poultry intestinal microflora and growth performance after feeding encapsulates through poultry diet.Objective 1 will formula of the encapsulation and methods will be optimized base on the releasing profile of essential compounds, and their effects on microbial. Microparticles will be produced using three types of technology, spray-drying, freeze-drying, and encapsulator. Objective 1 includes the following tasks:Task 1.1. Prepare water-soluble yellow mustard mucilage (WSM)Task 1.2. Prepare micro particles using Spray-DryingTask 1.3. Prepare microparticles using EncapsulatorTask 1.4. Prepare microparticles using Freeze-DryerTask 1.5. Evaluate encapsulation efficiency of essential oils and polyphenolsTask 1.6. Particle size measurementObjective 2 will evaluate the effect of micropaticles using in vitro methods in terms of releasing profile, delivery efficiency and effect on microbes. The tasks are listed below:Task 2.1. Digestion of the encapsulated compounds in vitroTask 2.2. Releasing profile Delivery efficiencyTask 2.3. Minimum inhibitory concentration (MIC) for microparticles by in vitro testObjective 3 will Evaluate poultry intestinal microflora and performance after feeding encapsulates through poultry diet. The encapsulated particles will be evaluated in chicken through diet. The study contains three major tasks: 1) microflora evaluation, 2) poultry performance measurement, and 3) delivery efficiency of the microparticles. The experimental plan is listed in Table 3. An antibiotic, clistin, will be used to compare with the encapsulated antibiotic alternatives at various concentrations. The taskes are listed below:Task 3.1 Set up the in vivo experiment: Task 3.2: Retention rate: Task 3.3. Effect of micro particles on intestinal microflora in chickenTask 3.4. Delivery efficiency of encapsulates in intestineTask 3.5. Poultry performance
Project Methods
Methods for objective 1: Formula of the encapsulation and methods will be optimized base on the releasing profile of essential compounds, and their effects on microbial. Microparticles will be produced using three types of technology, spray-drying, freeze-drying, and encapsulator.Statistical Analysis: Each experiment will be repeated three times. Data will be presented as Mean ± SD. Statistical computations will be performed using the GLM procedure of the Statistical Analysis System (SAS Release 9.3, SAS Institute Inc., Cary, NC, USA). The data for encapsulation efficiency and particle size prepared by the 3 different techniques will be examined using ANOVA. Least square means of each of the property factors will be calculated using the option of LSMEANS and statistical differences among the 3 techniques will be identified at p < 0.05 using the option of PDIFF.Methods for objective 2: This objective will evaluate the effect of micropaticles using in vitro methods in terms of releasing profile, delivery efficiency and effect on microbes.Statistical Analysis: Each experiment will be repeated three times. All values will be expressed as Mean ± SD. Mean values will be compared among treatment groups by ANOVA and subsequent Duncan's multiple range test employing SAS software (SAS Version 9.4, SAS Institute Inc., Cary, NC). Differences among means will be considered statistically significant at p < 0.05.Methods for objective 3: The encapsulated particles will be evaluated in chicken through diet. The study contains three major tasks: 1) microflora evaluation, 2) poultry performance measurement, and 3) delivery efficiency of the microparticles. Statistical analysis: All values will be expressed as Mean ± SD. Mean values will be compared among treatment groups by ANOVA and subsequent Duncan's multiple range test employing SAS software (SAS Version 9.4, SAS Institute Inc., Cary, NC). Differences among means will be considered statistically significant at p < 0.05.Ileum and cecal bacterial burden recovered from individual chickens between comparison groups will be evaluated using unpaired t-test by the GraphPad Prism version 6.00 (GraphPad Software, La Jolla, CA, USA, www.graphpad.com). This method can identify over 100 bacteria stains, which will help us to analyze the potential microflora change among treatment groups.Evaluations:1) Each experimental objective is achieved within the planned time frame; 2) Research findings will be disseminated in real time to the general public; 3) The technologies for producing microparticles of antimicrobial alternatives will be shared with other research scientists and poultry growers, feed producers through publications, presentations, educations and collaborations; 4) Up to 7 articles will be published in scientific journals by faculty and students;5) The quality and number of students trained on this project. About 8 students (2 M.S., and 6 B.S.) will complete their dissertation, thesis or senior projects using results generated from this project. Those students must maintain above 3.0 GPA and they will present their research at seminars or conferences.Evaluation Framework: Our project evaluation plan consists of six core assessments and will be monitored by Dr. Reddy, the Dean of the College as indicated by his Letter of Support.1) Self-evaluation within the research team: A quarterly progress report prepared by each PI will be shared with team members. This will allow the team to determine if the objectives are accomplished within the timeframe, and make adjustments in case of pitfalls;2) Institutional evaluation: Every TSU participant will present his (her) research at least once a year to the TSU family, and receive feedback from the faculty and students;3) Evaluation from the industrial partners: We will post project activities on the project website to receive comments from the 'Stake holders';4) Contributions from student research participants: All the junior scientists will submit weekly work reports to their supervisors, and their work will be evaluated by the major professor;5) Input/Project Oversight from ADM and UC Davis: On the second year of the project, Dr. Li from ADM will visit TSU campus to evaluate the project and make recommendations for improvements; Dr. Zhou from UC Davis will visit the TSU campus to give recommendations and technical guidance when the poultry experiment will start (as shown in Letter of Support from Dr. Li and Dr. Zhou),6) Social impact: Developing a tracking system of employment for all students receiving training on this project; citations of the articles and protocols (the top 10 most-read articles) and the visitor times of project websites.

Progress 02/15/19 to 02/14/23

Outputs
Target Audience:The results of this research was presented to the international conference, and has reached over 100researchers. The project results were also delivered to the classroom for undergraduate and graduate students training, and has reached over 150 students at Tennessee State Unviersity. Results and presentations were delivered to over 20 food and feed industries. Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided?Two (2) master students were trained and graduated from this project. They both obtained skills on encapsulation technologies, evaluating nanomaterials in terms of particles properties and delivery performance of particles. How have the results been disseminated to communities of interest?The presents were preseted in international conferences, going to be published in scientific journals, and presented in classrooms and to food industrial collaborators. What do you plan to do during the next reporting period to accomplish the goals? Nothing Reported

Impacts
What was accomplished under these goals? THe project has accomplished the following: Objective 1: formula of the encapsulation and methods will be optimized base on the releasing profile of essential compounds, and their effects on microbial. Microparticles will be produced using three types of technology, spray-drying, freeze-drying, and encapsulator. Under this project, the encapsulation formula was optimized after in vitro measuring theReleasing profile Delivery efficiency Minimum inhibitory concentration (MIC) for microparticles by in vitro tests. Objective 2:Evaluated the effect of micropaticles usingin vitromethods in terms of releasing profile, delivery efficiency and effect on microbes. Objective 3: Evaluated the poultry intestinal microflora and performance after feeding encapsulates through poultry diet. The encapsulated particles were evaluated in chicken through diet.

Publications

  • Type: Journal Articles Status: Submitted Year Published: 2023 Citation: Application of Yellow Mustard Mucilage in Encapsulation of Essential Oils and Polyphenols using Spray Drying


Progress 02/15/21 to 02/14/22

Outputs
Target Audience:The results of this research werepresented atinternational conferences, and havereached over 80 researchers. The project results were also delivered to the classroom for undergraduate and graduate students training, and havereached over 50 students at Tennessee State University. The generated work from this project was published in peer reviewed journals which has reached at least 200 people. Changes/Problems:Covid-19 has interupted the experimental progress, and the tornado in March 2020 has damaged the poultry farm. The experiment was delayed. Therefore the project was extended at no-cost for 1 additonal year and will end in Feb14, 2023. What opportunities for training and professional development has the project provided?Students were trained on formulatiingmicroparticles on a large scale, and experimental design for poultry trials. Students were also trained on giving presentations in conferences, writing manuscripts for publication, and collecting samples from poultry intestinal tracts. How have the results been disseminated to communities of interest?The results were disseminated by presentations in conferences. What do you plan to do during the next reporting period to accomplish the goals?The overall project will be completed in the next reporting period, and 2-3 manuscript will be submitted to peer reviewed journals.

Impacts
What was accomplished under these goals? The following tasks were accomplished: Task 3.1 Set up the in vivo experiment Task 3.2: Retention rate Task 3.5. Poultry performance

Publications

  • Type: Journal Articles Status: Published Year Published: 2021 Citation: Charles, P.R.A., Jin, T.Z., Mu, R., Wu, Y.*( 2021) Electrohydrodynamic processing of Natural polymers for active food packaging: A comprehensive review. Comprehensive Reviews in Food Science and Food Safety, DOI: 10.1111/1541-4337.12827.
  • Type: Journal Articles Status: Published Year Published: 2021 Citation: Wang, P., Wu, Y.* (2021) A Review on Colloidal Delivery Vehicles Using Carvacrol as A Model. Food Hydrocolloids, https://doi.org/10.1016/j.foodhyd.2021.106922


Progress 02/15/20 to 02/14/21

Outputs
Target Audience:The results of this research was presented to the international conference, and has reached over 50 researchers. The project results were also delivered to the classroom for undergraduate and graduate students training, and has reached over 100 students at Tennessee State Unviersity. 2019 Wu, Y.* Microencapsulation of antibiotic alternatives to modulate microflora. (Invited speaker, oral presentation). ACS (American Chemical Society) National Meeting, San Diego CA, August 2019. Changes/Problems:The biggest challenge is the feasibility of working on the in vivo test on poultry. Due to the severe tornano On March 4, 2020, the poutry farm in Tennessee State University was completed damaged leaving a flattened poultry barn in the farm. The COVID 19 after this tornado has halted many construction process, and limited the research activities for the PI and the student. There is no farm facility to conduct the poultry experiemtns. The alternative solution are sought to continure the project. The interstinal content of poultry collected from the co-PI, Dr. Nahashon, before the tornano will be used to evaluate the antimicrobial effects on the microparticles. We are in the process of addressing the research protocols. What opportunities for training and professional development has the project provided?The graduate student working on this project has been trained in experiemental skills on chemical, physicochemical and microbial research, including spectrophotometric analysis, viscosity analysis, zeta-potential measurement, microbiological tests, encapsulation using spray drying, and writing scientific reports, data analysis using SAS, presentations, and manuscript preparation. How have the results been disseminated to communities of interest?Yes. The results were presented in the ACS national conference, and was submitted to IFT annual conference. What do you plan to do during the next reporting period to accomplish the goals?More physicochemical properties of the encapsulated microparticles will be evaluated using FT-IR, and stability of the particles will also be evaluated.

Impacts
What was accomplished under these goals? Under Objective 1) Formulate and optimize microencapsulation for antibiotic alternatives, the following tasks has been completed: Task 1.1. Prepare water-soluble yellow mustard mucilage (WSM) Task 1.2. Prepare micro particles using Spray-Drying Task 1.5. Evaluate encapsulation efficiency of essential oils and polyphenols Task1.6. Particle size measurement Under Objective 2) Investigate the delivery efficiency, releasing profile and effects on bacteria of the microparticle usingin vitromethods, the following tasks has been completed: ? Task2.1. Digestion of the encapsulated compounds in vitro Task2.2. Releasing profile Delivery efficiency Task 2.3. Minimum inhibitory concentration (MIC) for microparticles by in vitro test

Publications

  • Type: Conference Papers and Presentations Status: Published Year Published: 2020 Citation: 2019 Wu, Y.* Microencapsulation of antibiotic alternatives to modulate microflora. (Invited speaker, oral presentation). ACS (American Chemical Society) National Meeting, San Diego CA, August 2019.


Progress 02/15/19 to 02/14/20

Outputs
Target Audience:This project aims to reach over 500 people through scientific presentations, journal publications, and classroom teaching. Detailed health benefits of antibiotic alternatives will be transferred to audiences and feed manufactures. Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided?Two students are recruited. THe students are trained with corresponding skillsets on polysaccharide research, fractionation and characterization of polysaccharides using tensiometer, rheometer, size exclusion chromatography, and extraction and purification of polysaccharides. How have the results been disseminated to communities of interest? Nothing Reported What do you plan to do during the next reporting period to accomplish the goals?Objective 1, task 1.2-1.5 will be completed during next reporting period.

Impacts
What was accomplished under these goals? Objective 1, task 1 is accomplished. Objective 1 will formula of the encapsulation and methods will be optimized base on the releasing profile of essential compounds, and their effects on microbial. Microparticles will be produced using three types of technology, spray-drying, freeze-drying, and encapsulator. Objective 1 includes the following tasks: Task 1.1. Prepare water-soluble yellow mustard mucilage (WSM)

Publications