Source: UNIV OF MARYLAND submitted to NRP
UNDERSTANDING MECHANISMS OF CHANGES IN RUMINAL METABOLISM
Sponsoring Institution
National Institute of Food and Agriculture
Project Status
COMPLETE
Funding Source
Reporting Frequency
Annual
Accession No.
1014972
Grant No.
2018-67015-27493
Cumulative Award Amt.
$493,000.00
Proposal No.
2017-05882
Multistate No.
(N/A)
Project Start Date
Jan 15, 2018
Project End Date
Jan 14, 2025
Grant Year
2018
Program Code
[A1231]- Animal Health and Production and Animal Products: Improved Nutritional Performance, Growth, and Lactation of Animals
Recipient Organization
UNIV OF MARYLAND
(N/A)
COLLEGE PARK,MD 20742
Performing Department
(N/A)
Non Technical Summary
Cattle convert crops like grass and food byproducts to high-quality protein like milk and meat. Microorganisms that live in the cow's first stomach chamber, called the rumen, initially digest these feeds, and the cow lives on the byproducts of the digestion and the microbes themselves. However, this digestion and fermentation process also releases methane gas, which represents a loss of 2% to 10% of the energy in the diet, and it is a potential greenhouse gas. The goal of the proposed research is to improve the way digestion occurs in the cow's rumen to decrease methane emissions and to thereby increase the efficiency and improve the environmental impact of food production from available feeds. The overarching hypothesis for this research is that mathematical models of fermentation based on classical laws of physics can explain and predict the profile of end products from fermentation in the cow's rumen. Specific objectives include studying the way different nutrients and probiotics in the diet cause shifts in metabolism based on laws of physics. We expect this research to show how to regulate different fermentation pathways to improve efficiencies of production and health, and ultimately to identify ways to decrease wasteful methane emissions from cattle. Results will be used to improve ration formulation for cattle, and to predict energy and protein availability for different feeds.
Animal Health Component
15%
Research Effort Categories
Basic
85%
Applied
15%
Developmental
(N/A)
Classification

Knowledge Area (KA)Subject of Investigation (SOI)Field of Science (FOS)Percent
30234101010100%
Goals / Objectives
The goal of the proposed project is to develop and communicate an improved understanding of the mechanisms causing changes in ruminal fermentation that affect the profile of volatile fatty acids (VFA) and gases (carbon dioxide, methane and hydrogen).The primary objectives will be: 1) determine the effects of several enzyme inhibitors on enzyme kinetics and thermodynamics; 2) determine variation in enzyme kinetics and thermodynamics due to diurnal variation, type of diet, and transition from one diet to another; 3) correlate metagenomic and metatranscriptomic measurements with ruminal fluid microbial activity; 4) develop a dynamic mechanistic model incorporating data collected in the proposed project; and 5) this research will be available to disseminate to research, extension, and academic audiences using the developed computer models as tools.
Project Methods
Both in vitro and in vivo methods will involve measurements of VFA and gas production in small samples of ruminal fluid immediately after sampling. Ruminal fluid will be sampled directly into centrifuge tubes, which will be stoppered as they are removed to prevent changes in gas composition. Generally, 10 ml of ruminal fluid will be incubated in sealed 15-ml tubes with initial gas headspace filled with rumen gases at sampling. A hypodermic needle attached to a gas-tight syringe will be inserted through the stopper to quantify and collect produced gases. Intentionally, this method does not allow time for the ruminal fluid to change appreciably (e.g. pH become much lower), or for the activity of the microbial population to change. Thus, results will represent the instantaneous velocity of the reactions at the time the sample is taken.3.3 VFA and gas measurementsThe liquid samples will be analyzed without derivatization by a gas chromatograph (GC) with FID detector using a packed column for acetate, propionate, butyrate, isobutyrate, valerate, and isovalerate. The gases CO2, CH4, H2, and N2 will be collected in gas-tight syringes and measured directly on a GC with thermal conductivity detector. N2 gas will be an indicator of leakage.Isotope enrichment will be measured on selected samples by Dr. Nishanth Sunny. An isotope ratio mass spectrometer (IRMS) coupled to a gas chromatograph (GC) via a combustion oven (comb) will be used to measure enrichments. VFA will be introduced using a solid phase micro extraction method (Yo, 1999). CO2 and CH4 enrichment will also be determined on this machine as described by Ai et al. (2013) This device has lower limits of detection below 0.001% enrichment.3.4 Perturbation experimentsThe rates of methane and VFA production, and VFA interconversion will be measured, with addition of 5 levels of different substrates including: H2, CO2, D-glucose, sodium salts of acetate, succinate, lactate, propionate and butyrate, for a total of 40 tubes in addition to the 2 tubes with no additions. Samples with added gases will be fermented under pressure, but other samples will be fermented at atmospheric pressure by allowing attached syringes to expand.3.5 Calculation of deltaG in ruminal fluidThe deltaG for production from glucose and interconversion of each end product (CO2, H2, Acetate, Propionate, Butyrate, Lactate, and Succinate, etc.) will be calculated for both in vitro and in vivo experiments according to established equations (e.g. Ungerfeld and Kohn, 2006)3.6 Calculation of Vmax and Km Data collected from the perturbation experiment in Section 3.4 will be used to calculate apparent Vmax and Km for all production and interconversion pathways between substrates and products. The Vmax and Km will be determined by regression of the inverse of initial substrate by the response plotted as the inverse of the initial velocity; slope = Vmax/Km and X intercept = -Km-1 in accordance with Lineweaver-Burk plots.3.7 In vitro experiments with inhibitorsThe deltaG, Vmax and Km will be determined as described above for ruminal fluid taken 4 hours after feeding and used to determine kinetic and thermodynamic parameters with or without addition of one of two-levels of the following inhibitors: ionophore, pH, NO3, and SO3.3.8 In vivo experiment The proposed experiment will be conducted with 4 rumen-cannulated late-lactation or non-lactating Holstein cows in a double switchback design. Treatments will be two different forage:concentrate ratios (100% forage and 70:30) by substituting corn grain for timothy hay. Samples will be taken on days 2, 9, and 21 at 4-hours after feeding for each of the 4 periods. The earlier samples will show changes during transition from one diet to the other. On the 21st day of each treatment, samples will also be taken at 1, 8, and 16 hours after morning feeding, as well as 4 hours after feeding as indicated. Thus, treatments will represent different forage to concentrate ratios, transitions from one diet to the other, and diurnal variation.Stable isotopes will be used for additional measurements. Stable 15N-NH4+ will be added to two duplicate samples without any other additions to measure microbial growth on each treatment. Stable 13C-label will be used to show the specific conversion from added substrate to major end products. Thus, these results will show Vmax for specific conversions of each added substrate to the possible end products. The specific Vmax will show which pathway steps are affected by treatments.3.9 Metagenomics and metatranscriptomicsThe samples taken on day 21 will be composited over the 4 time points for each cow and period and analyzed for metagenomic and metatranscriptomic differences between the 8 observations of animals on high-concentrate diets and the 8 observations on high-forage diets. In addition to descriptive analysis of the populations and transcriptome, 16S r-RNA analysis will be used to quantify shifts in populations involved in alternative pathways for propionate synthesis (e.g. lactic acid bacteria vs. succinic acid bacteria), and changes in gene expression for production and utilization of lactic acid and succinate will be determined. Changes in quantity of methanogens, and reductive acetogens, and the transcripts for the processes they carry out will also be determined.3.10 Development of a mechanistic modelThe in vitro and vivo experiments will be used to develop a mathematical model incorporating the kinetic and thermodynamic parameters. Data will be collected for rates and ?G for production and interconversion of each major VFA (acetate, propionate, butyrate, succinate, and lactate). VFA production from glucose or CO2 and H2 will be quantified. All kinetic and thermodynamic parameters will be calculated for pathways to and from pyruvate, the central intermediate for most VFA production by solving simultaneously using the data representing overlapping pathways. A compartmental model will be fit using the variables of deltaG, Km, and Vmax for each set of conditions (e.g. high forage or high concentrate, tested inhibitors), and then the variables will be adjusted for different types of diets. This adjustment can also be predicted mechanistically from the energy obtained by organisms that carry out certain reactions. For example, as more substrate is metabolized in a specific pathway, organisms that carry out the pathway would grow and their activity would increase. If deltaG becomes very negative because of low product concentration, higher growth rates may be predicted. For example, methanogen growth rate increases as deltaG becomes more negative. Since changes in Vmax and Km that are predicted mechanistically are likely to be less accurate than empirically predicted parameters, an alternative model will use force functions for setting these parameters for different types of diets. Both models will later be tested for prediction accuracy compared with published studies. Generally, more empirical models are more accurate, but provide less information to test potential mechanisms of metabolism control. However, the more empirical model is likely to be more readily applicable in the field for desired predictions. The dynamic models will be developed using the software ScientistTM from Micromath Corp and demonstrated for teaching using StellaTM.

Progress 01/15/18 to 01/14/25

Outputs
Target Audience:The target audience was primarily animal nutritionsts as researchers and practitioners. Results were presented in abstracts and refereed articles and extension talks. Changes/Problems:Covid pandemic presented the major problems with this study. It was delayed due to inability to conduct the research during the early part of the study. Subsequently, University administrative practices add complexity toconducting research due to delays, miscommunications, arbitrary changes in rules, changes in software used, and reporting methods. The IACUC has been excellent. What opportunities for training and professional development has the project provided?Three Ph.D. students and one M.S. degree student were trained on aspects of this study. How have the results been disseminated to communities of interest?Yes, results were presented at national meetings of the American Society of Dairy Science and communicated directly to interested investigators. What do you plan to do during the next reporting period to accomplish the goals? Nothing Reported

Impacts
What was accomplished under these goals? Several in vitro studies and two in vivo studies with fistulated cows were conducted. Major pathways that can be regulated via factors that affect kinetics or thermodynamics were identified. Studies confirmed which ruminal pathways are regulated by thermodynamics and when that regulation shifts.

Publications

  • Type: Peer Reviewed Journal Articles Status: Published Year Published: 2022 Citation: Li, M. M., S. Ghimire, B. A. Nenner, R. A. Kohn, J. L. Firkins, B. Gill, M. D. Hanigan.2022. Effects of acetate, propionate, and pH on volatile fatty acid thermodynamics in continuous cultures of ruminal contents. J. Dairy Sci. 105 (11), 8879-8897.
  • Type: Peer Reviewed Journal Articles Status: Published Year Published: 2022 Citation: Liu, J., Y. Bai, F. Liu, R. A. Kohn, D. A. Tadesse, S. Sarria, R. W. Li, and J. Song 2022. 10.3390/ani12212995 Animals, 12, 2995.


Progress 01/15/23 to 01/14/24

Outputs
Target Audience:The target audience includes scientists and professional nutritionsits. Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided?This year one Ph.D. student worked on this project and one undergraduate student. How have the results been disseminated to communities of interest?Results were presented at national meetings of the American Dairy Science Association. What do you plan to do during the next reporting period to accomplish the goals? Nothing Reported

Impacts
What was accomplished under these goals? Project was completed and the last in vivo trial was initiated and is underway. It will be completed using additional resources.

Publications


    Progress 01/15/22 to 01/14/23

    Outputs
    Target Audience:Farmers, studetns, government advisors, and animal nutrition consultants. Changes/Problems:The biggest problem was the Covid pandemic which prevented the first Ph.D. student from completing all of the planned experiments before graduating. In addition, this caused a personnel issue as my technician left for a different job because of the limitations. While we have recovered from those setbacks, they had left us behind schedule. What opportunities for training and professional development has the project provided?We have employed two undergraduate students in the laboratory and one graduate student. We have had two international visiting students from Colombia and Nigeria. In addition, I teach graduate student research presentations and seminar where results are shared. How have the results been disseminated to communities of interest?Results have been incorporated in educational extension materials developed routinely. What do you plan to do during the next reporting period to accomplish the goals?A PhD student graduated last year and a new student has initiated a new project that will use techniques we developed to investigate effects of methane inhibitors on overall kinetics and thermodynamics.

    Impacts
    What was accomplished under these goals? As can be seen by the listed publications, we continued to elucidate limiting pathways in rumen fermentation contributing to utilization of substrate to produce energy for the animal and the byproduct methane that is eructated from the rumen.

    Publications

    • Type: Journal Articles Status: Published Year Published: 2021 Citation: Sale, N. A., R. A. Kohn, A. Saleh, D. D. Yusuf, O.A. Lawal, S.I. Idris. 2021. Determinations of some Typha mineral composition and organic loading rate for anaerobic digestions. J. Agric. Engineer. Technol. 26 (2), 27-43.
    • Type: Journal Articles Status: Published Year Published: 2022 Citation: *Sale, N. A., R. A. Kohn, A. Sale, U. S. Mohammed, I. B. Dalha. 2022. Composition and biochemical methane potential from different Typha components. Arid Zone J. Engineering, Technol. Environ. 18 (4), 611-622.
    • Type: Journal Articles Status: Published Year Published: 2022 Citation: Liu, J., Y. Bai, F. Liu, R. A. Kohn, D. A. Tadesse, S. Sarria, R. W. Li, and J. Song 2022. Rumen Microbial Predictors for Short-Chain Fatty Acid Levels and the Grass-Fed Regimen in Angus Cattle. Animals, 12, 2995.
    • Type: Journal Articles Status: Published Year Published: 2022 Citation: Li, M. M., S. Ghimire, B. A. Nenner, R. A. Kohn, J. L. Firkins, B. Gill, M. D. Hanigan.2022. Effects of acetate, propionate, and pH on volatile fatty acid thermodynamics in continuous cultures of ruminal contents. J. Dairy Sci. 105 (11), 8879-8897.


    Progress 01/15/21 to 01/14/22

    Outputs
    Target Audience:Continue to support scientists, students, farmers, government advisors, and animal nutrition consultants. Changes/Problems:Research continued to be impacted by COVID-19 restrictions and requirements to decrease occupancy of the laboratory. What opportunities for training and professional development has the project provided?Training of graduate students continued including Jarvis Scott and Elizabeth Rendon (from University of MedeĆ­n,Columbia). How have the results been disseminated to communities of interest?Abstracts were submitted online, popular articles written for Lancaster Farmer, field day presentation for Central Maryland Research and Education Center. What do you plan to do during the next reporting period to accomplish the goals?We plan to complete the in vivo trial and publish results.

    Impacts
    What was accomplished under these goals? In vitro studies on enzyme kinetics were continued. Initial studies evaluated reaction rates when hydrogen gas was infused from physiological to greater than physiological levels. Subsequent studies varied the amount of fatty acids and intermediates. In vivo study to evaluate changes in ruminal activity was initiated, and half completed. However, the second half (two periods) could not be completed prior to scheduled non-lactating period before calving. Thus, the same cows will be used this spring after calving.

    Publications

    • Type: Conference Papers and Presentations Status: Published Year Published: 2020 Citation: Rendon, M. E., S. L. Rattiff, J. McDermott, J. Scott, R. Rha, and R. A. Kohn. 2020. Effect of nitrate and hydrogen addition on methane production in vitro. J. Dairy Science Supplement 103: 202.
    • Type: Conference Papers and Presentations Status: Published Year Published: 2020 Citation: Scott, J. and R. Kohn. 2020. Kinetics of methanogenesis and acetogenesis under normal rumen conditions. J. Animal Science Supplement 97(3): 243
    • Type: Conference Papers and Presentations Status: Published Year Published: 2020 Citation: Rha, Y., S. L. Ratiff, J. S. Scott, and R. A. Kohn. 2019. Effect of air and probiotics on in vitro fermentation. J. Dairy Science Supplement, 102(1):19.


    Progress 01/15/20 to 01/14/21

    Outputs
    Target Audience:Target audience included scientists and members of the public. Changes/Problems:Our laboratory was decreased to a low number of personnel due to COVID-19 pandemic. This has resulted in a delay in research accomplishments as the number of undergraduate students working in the lab was greatly reduced. What opportunities for training and professional development has the project provided?Jarvis Scott continued Ph.D. studies. How have the results been disseminated to communities of interest?Talks given to scientis andnon-scientist audiences. What do you plan to do during the next reporting period to accomplish the goals?Continue in vivo experiment to evaluate differences in rumen microbial activity (enzyme kinetics and thermodynamics).

    Impacts
    What was accomplished under these goals? Continued research on enzyme kinetics and thermodynamics. Completed surgeries for rumen fistulas for 5 cows. Collected preliminary data.

    Publications


      Progress 01/15/19 to 01/14/20

      Outputs
      Target Audience: Target audience was generally scientists with presentations at national research conferences. A seminar was presented on related technology at the Polytechnic University of Madrid, Spain. Presented to AAAS Fellows in Washington DC.Presentations were made to students and community groups on animal production and climate change. Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided?Rachel Rha received her Master of Science Degree during this time period. Jarvis Scott contined work toward his Ph.D. degree. How have the results been disseminated to communities of interest?There were addtional talks provided to audiences regarding the impact of animal agriculture on climate change, with particular emphasis on green house gas (e.g. methane) emissions. Audiences included policy makers and advisors (e.g. AAAS Fellows), international scientists and farmers (e.g. US, India, and Nigeria). What do you plan to do during the next reporting period to accomplish the goals?Continue to refine techniques to measure enzyme kinetics and thermodynamics in vitro to evaluate changes in rumen fluid activity.

      Impacts
      What was accomplished under these goals? In 2019, work continued on objective 1 "determine the effects of several enzyme inhibitors on enzyme kinetics and thermodynamics." Nitrate inhibition was tested and shown to be largely caused by indirect effects from decreasing hydrogen gas substrate. Toward objectives 2-3, methods were developed for testing ruminal fluid changes on different types of diets. ONe modely regarding objective 4 was amechanistic model of gas flows was developed as part of a Master of Science Degree.

      Publications

      • Type: Conference Papers and Presentations Status: Published Year Published: 2019 Citation: Kohn, R. A. 2019. Opportunities to mitigate greenhouse gases from agriculture. Beyond Electricity: Climate Change and the 75% Program. June 28, 2019. Conference for AAAS Fellows, Washington, DC.


      Progress 01/15/18 to 01/14/19

      Outputs
      Target Audience:Target audience was generally scientists with presentations at national research conferences. A field day explaining research to farmers at a field day was also performed. Changes/Problems:No major challenges initially. What opportunities for training and professional development has the project provided?Rachel Rha completed a MS degree in 2020. Experimental supplies were funded by the project, assistantship by Department. Postdoctoral faculty associate, Shiron Rattiff, who was funded by the project has taken a position at NIH. Ph.D. Student Jarvis Scott continues to conduct research on the project. How have the results been disseminated to communities of interest?So far results were distributed by abstracts and other procedings and a field day at the Central Maryland Research and Education Center. What do you plan to do during the next reporting period to accomplish the goals?We intend to complete the long-term animal study measuring kinetic parameters in fistulated cows on different diets in February, within this study are enzyme kinetics with and without stable isotopes, and metagenomics studies. Then complete modelling and writing up of results.

      Impacts
      What was accomplished under these goals? During the progress period, experiments were conducted on enzyme kinetics and thermodynamics in vitro, and methods to analyze rumen fluid for enzyme activity were completed and evaluated.

      Publications

      • Type: Journal Articles Status: Published Year Published: 2018 Citation: Judd, L. and R. A. Kohn. 2018. Test conditions that affect in vitro production of volatile fatty acids and gases. J. Anim. Sci. 96:694-704.
      • Type: Conference Papers and Presentations Status: Published Year Published: 2019 Citation: Rha, Y., S. L. Ratiff, J. S. Scott, and R. A. Kohn. 2019. Effect of air and probiotics on in vitro fermentation. J. Dairy Science Supplement, 102(1):19.