Progress 10/01/15 to 09/30/20
Outputs Target Audience:Target audience of our research include: The Food Science community The Cereal Science community Agricultural Science community Food product developers Cereal product developers The education community Food / Cereal industry Bio macromolecule community Imaging community Cereal science equipment manufacturers General scientific community Food safety community Food industry Entrepreneurs Changes/Problems:
Nothing Reported
What opportunities for training and professional development has the project provided?Over the course of the past year three PhD students have graduated from the Kokini Laboratory and, two MS students from Mishra lab, andone PhD and two MS from Huang Lab, all of whom have continued on in their careers in research. Additionally, we have had six undergraduate students performing research, and the most recent graduate has now entered her master's program at Cornell University. Outside of this, students have been able to attend conferences and compete in a variety of competitions relevant to their respective areas of research. We also trained over 100 industry and regulatory agency professionals in the area of food processing andfood safey, through the extension program of Mishra Lab. How have the results been disseminated to communities of interest?The primary method of disseminating information to the community is through publication in journals. We have also attended conferences such as the Institute of Food Technology, Cereals and Grains, the American Society of Baking, and the Society of Rheology. By going to these conferences, we further share the discoveries made in our laboratory. We have also provided extension publications for the stakholders. What do you plan to do during the next reporting period to accomplish the goals?
Nothing Reported
Impacts What was accomplished under these goals?
Since the beginning of 2019, the Kokini laboratory has collectively published 27 papers in reputable journals throughout the world, including 11 since the start of 2020. Our research has progressed the field of cereal science by developing a method of site click chemistry to attach quantum dots to antibodies raised against the primary protein components of wheat. This has allowed for the development of novel visualization techniques that have not been linked to rheological data as well. Dough research has also been advanced through our development of LAOS rheology, allowing for a more in-depth characterization of wheat dough in the various parts of mixing, and this technology is also being applied to dairy products such as cheese and yogurt. We have also developed nano particles and nano tubes by generating deeper understanding of electrostatic surface interactions of proteins. This has led to the development of particles that are able to survive in the harsh conditions of the digestive track and deliver curcumin to the lower parts of the digestion track. We have also developed novel films from kaffirin and zein, products that are currently waste streams. These films offer the potential to serve as components of biodegradable plastics for the food industry. Lastly we have developed a number of biosensors through the use of electrospinning. These high surface area mats are decorated with gold nanoparticles which enhance the detection limits of various analytes, such as acrylamide, when using RAMAN spectroscopy. Related to this work is the development of gliadin sensors that do not use the harsh chemicals traditionally associated with detecting these substances. The defining link in all of this work is a strong focus on food chemistry and materials characterizations. As a lab we develop understanding of the physical chemistry of protein, starch, and lipids, and how those interact with one another. In doing this, we offer insight on a variety of different food industry applications, as is seen in the diversity of our research. Corvalan lab: In this reporting period we have continued to advance the mechanistic understanding of the physics of green cleaning methods using environmentally friendly products and procedures to reduce the chemical and water use during cleaning of processing equipment. We have disseminated this work in a collaborative publication: Mishra lab: We have continued to work on the novel food processing systems and development of non-invasive sensor for product monitoring during commercial food manufacturing. We have also developed the pilot scale novel MB CIP system that will reduce the water use in commercial CIP systems. Cold plasma inactivation of spore formers project is also beingn studied for deployment in a commercial manufacturing environment.
Publications
- Type:
Journal Articles
Status:
Published
Year Published:
2021
Citation:
Tsai, J.-H., Huang, J.-Y., Wilson, D.I. 2021. Life cycle assessment of cleaning-in-place operations in egg yolk powder production. Journal of Cleaner Production, 278, 123936.
- Type:
Journal Articles
Status:
Published
Year Published:
2020
Citation:
2. Rashid, F., Bao, Y., Ahmed, Z., Huang, J.-Y. 2020. Effect of high voltage atmospheric cold plasma on extraction of fenugreek galactomannan and its physicochemical properties. Food Research International, 138, 109776.
3. Bao, Y., Reddivari, L., Huang, J.-Y. 2020. Enhancement of phenolic compounds extraction from grape pomace by high voltage atmospheric cold plasma. LWT - Food Science and Technology, 133, 109970.
4. Bao, Y., Reddivari, L., Huang, J.-Y. 2020. Development of cold plasma pretreatment for improving phenolics extractability from tomato pomace. Innovative Food Science and Emerging Technologies, 65, 102445.
5. Zhang, B.Y., Xu, S., Villalobos-Santeli, J.A., Huang, J.-Y. 2020. Fouling characterization of camel milk with comparison to bovine milk. Journal of Food Engineering, 285, 110085.
6. Lu, J., Corvalan, C.M., Huang, J.-Y. 2020. Deformation and removal of viscous thin film by submerged jet impingement. AIChE Journal, 66, e16745.
- Type:
Journal Articles
Status:
Published
Year Published:
2019
Citation:
Zhang, B.Y., Tong, Y., Singh, S., Cai, H., Huang, J.-Y. 2019. Assessment of carbon footprint of nano-packaging considering potential food waste reduction due to shelf life extension. Resources, Conservation & Recycling, 149, 322-331.
- Type:
Theses/Dissertations
Status:
Accepted
Year Published:
2020
Citation:
1. Zhang, Y. 2020. Interactions among proteins and carbohydrates under thermal processing conditions and their effects on dairy fouling. Ph.D. dissertation, Department of Food Science, Purdue University.
2. Bao, Y. 2020. Title: Innovative Cold plasma-assisted extraction for bioactive compounds from agricultural byproducts. M.S. thesis, Department of Food Science, Purdue University.
3. Salazar Tijerino, M.B. 2020. Evaluation of the techno-economic and environmental performance of craft beer production: A case study on microbrewery. M.S. thesis, Department of Food Science, Purdue University.
- Type:
Theses/Dissertations
Status:
Accepted
Year Published:
2020
Citation:
1. Cantarero, F. (2020). Development of a non-intrusive continuous sensor for early detection of fouling in commercial manufacturing systems. M.S. thesis, Department of Food Science, Purdue University.
2. Mehta H. (2020). Design of complementary experiments for estimation of temperature-dependent thermal properties. M.S. thesis, Department of Food Science, Purdue University.
- Type:
Journal Articles
Status:
Published
Year Published:
2020
Citation:
1. Fernando, C., Mishra, D.K., Ozadali, F., 2020. Development of a non-intrusive continuous sensor (NICS) to estimate thermal conductivity of food products in closed system. Food and Bioproducts Processing, 123, 390-397.
2. Benyathiar, P., Selke, S.E., Harte, B.R., Mishra, D.K., 2020. The effect of irradiation sterlilization on poly(lactic) acid films. Journal of Polymer Degradation and Stability. Journal of Polymers and the Environment, 1-12.
3. Vidyarthi, S., Mishra, D.K., Muramatsu, Y., 2020. Inverse estimation of fluid to particle heat transfer coefficient in aseptuc processing of particulate foods. Biosystems Engineering. Biosystems Engineering 198, 210-222
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Progress 10/01/18 to 09/30/19
Outputs Target Audience: Food engineering and food science scientific community, Indiana stakeholders, food processors, individual entrepreneurs and small-scale businesses. Changes/Problems:
Nothing Reported
What opportunities for training and professional development has the project provided?Knowledge gained through the projects was used in the yearly workshops that are conducted at Purdue University Campus. How have the results been disseminated to communities of interest?Yes, this has been dissemienated through the training and workshops that are regularly conducted. What do you plan to do during the next reporting period to accomplish the goals?
Nothing Reported
Impacts What was accomplished under these goals?
Characterize multi-scale physical, chemical and biological properties of food, biological and engineered materials.Cold plasma was applied on grape pomace as pretreatment to enhance the performance of conventional solvent extraction methods for bioactive compounds. Grape pomace treated by helium plasma showed higher extraction yields of total phenolic compounds and anthocyanin. The extracts also had higher antioxidant activities. This plasma-assisted extraction technology can be used to valorize the waste/byproducts from grape processing more efficiently with lower environmental impacts. Multi-state project on the innovative solutions to thermal propoerties of food materials. Mylti-state project on the modeling and validation of low moisture food products.
Publications
- Type:
Book Chapters
Status:
Submitted
Year Published:
2019
Citation:
Anderson, N., Benyathiar, P., Mishra, D.K., 2019. Aseptic Processing. Food Process Engineering. Springer.
- Type:
Journal Articles
Status:
Published
Year Published:
2019
Citation:
Muramatsu, Y., Dolan, K.D., Mishra, D.K., 2019. Factors influencing estimation of thermal inactivation parameters in low-moisture foods using a test cell. Journal of Food Engineering 262, 100-108.
- Type:
Journal Articles
Status:
Published
Year Published:
2018
Citation:
Samsudin, H., Auras, R., Mishra, D., Dolan, K., Burgess, G., Rubino, M., Selke, S., Soto-Valdez, H., 2018. Migration of antioxidants from polylactic acid films: a parameter estimation approach and an overview of the current mass transfer models. Food Research International 103, 515-528.
- Type:
Conference Papers and Presentations
Status:
Other
Year Published:
2019
Citation:
Mishra, D.K. 2019. Aseptic design (piping/ valves/ engineering) with respect to regulations and guidance. IFTPS, San Antonio, TX, Feb. 26-28, 2019.
- Type:
Conference Papers and Presentations
Status:
Other
Year Published:
2018
Citation:
Mishra, D.K. 2018. Utilization of modeling tools for aseptic process optimization. Aseptipak, Dallas, TX.
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Progress 10/01/17 to 09/30/18
Outputs Target Audience: Food engineering and food science scientific community, Indiana stakeholders, food processors, individual entrepreneurs and small-scale businesses. Changes/Problems:
Nothing Reported
What opportunities for training and professional development has the project provided?The project has provided the following workshops: 1. Aseptic Processing and Packaging (3.5 days) - Attended by 72 industry professionals. 2. Food and Drug Administration Training (Total 4 trainings, each 5-day long) - Each training was attended by at least 28 FDA inspectors. 3. Better Process Control School (5-day course) - Attended by 35 industry professional. 4. Validation Workshop (3.5 days) - Attended by 24 industry professionals. How have the results been disseminated to communities of interest?The results have been disseminated by peer review articles in journals and workshop handouts and binders. What do you plan to do during the next reporting period to accomplish the goals?Plans for next reporting period: 1. Collaboration with other multistate stations, especially in the area of cold plasma work and high-pressure processing research. 2. An additional workshop on Inverse Problems that will be attended by international community involved with parameter estimation and inverse problems techniques.
Impacts What was accomplished under these goals?
Mishra with Dolan at Michigan Station: Resulted in NSF STTR Phase I grant $225K with Indiana matching funds $50K. Title: A Device for Rapid Estimation of Temperature Dependent Thermal Properties for Food Processing Systems. • The research of Dr. Huang's Food Process Sustainability lab focuses on: • (a) Fundamental studies in understanding mechanisms of formation and removal of food deposits, aiming to find potential mitigation methods toward reduced fouling in food processing • (b) Physical approaches for cleaning and disinfection in the food processing environment, aiming to develop optimally management of the clean-in-place process to minimize water and chemicals consumption • (c) Applications of an electro-membrane process for biomass valorization, including fractionation of bioactive peptides fish byproducts and removal of acetic acid from corn stover hydrolysate • Dr Corvalan group's research, in collaboration with Dr. Campanella's group, has led to: Fundamental research at thenanoscale Dr.Jozef Kokini group's research is focussed on the manufacturing of nanoparticles and its applications. 1:Advancing the fundamental science and application of technologies to ensure food safety and improve quality of food products 1a. Utilize innovative methods to characterize food materials • Temperature dependent thermal properties measurement device TPCell 1b. Develop new and improved processing technologies • Mishra with Indiana stakeholders • Huang, Mishra and Corvalan for improved CIP with less chemical use and improved sustainability for food production facilities 1c. Develop mathematical models to enhance understanding of, and optimize food processes • Mishra with the advancement in understanding of rapid cooling through mathematical model • Optimization of thermal processes with temperature dependent thermal properties 2:Develop pedagogical methodologies for improved learning of food engineering principles. 2a. 3:Develop outreach programs to disseminate best practices for enhancing food safety and quality to stakeholders. 3a. Workshop on aseptic processing and packaging 3b. Workshop on validation of aseptic processing and packaging
Publications
- Type:
Journal Articles
Status:
Published
Year Published:
2018
Citation:
Rouf T. B., Schmidt G., and Kokini J. L. (2018) Zein-Laponite nanocomposites with improved mechanical, thermal and barrier properties. Journal of Materials Science. 53, 7387-7402 https://doi.org/10.1007/s10853-018-2061-6
- Type:
Journal Articles
Status:
Published
Year Published:
2018
Citation:
Maldonado, L., and Kokini, J. L. (2018). An optimal window for the fabrication of Edible Polyelectrolyte Complex Nanotubes (EPCNs) from bovine serum albumin (BSA) and sodium alginate. Food Hydrocolloids. Vol 77, 336-346
- Type:
Journal Articles
Status:
Published
Year Published:
2017
Citation:
Maldonado, L., Sadeghi, R., and Kokini, J. L. (2017). Nanoparticulation of bovine serum albumin and poly-d-lysine through complex coacervation and encapsulation of curcumin. Colloids and Surfaces B: Biointerfaces. 159:759-769
- Type:
Journal Articles
Status:
Published
Year Published:
2018
Citation:
Lu, Jiakai, Diego M. Campana, and Carlos M. Corvalan. "Contraction of surfactant-laden pores." Langmuir 34.15 (2018): 4701-4706.
- Type:
Journal Articles
Status:
Published
Year Published:
2018
Citation:
Hayati Samsudin, Rafael Auras, Dharmendra Mishra, Kirk Dolan, Gary Burgess, Maria Rubino, Susan Selke, Herlinda Soto-Valdez,
Migration of antioxidants from polylactic acid films: A parameter estimation approach and an overview of the current mass transfer models,
Food Research International,
Volume 103, 2018
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Progress 10/01/16 to 09/30/17
Outputs Target Audience:Food engineering and food science scientific community, Indiana stakeholders, food processors, individual entrepreneurs and small-scale businesses. Changes/Problems:
Nothing Reported
What opportunities for training and professional development has the project provided?
Nothing Reported
How have the results been disseminated to communities of interest?
Nothing Reported
What do you plan to do during the next reporting period to accomplish the goals?
Nothing Reported
Impacts What was accomplished under these goals?
i. Main accomplishments (do not include figures and tables) See "Collaborations" ii. Collaborations (stations/members) Mishra with Dolan at Michigan Station: Resulted in NSF STTR Phase I grant $225K with Indiana matching funds $50K. Title: A Device for Rapid Estimation of Temperature Dependent Thermal Properties for Food Processing Systems. The research of Dr. Huang's Food Process Sustainability lab focuses on: (a) Fundamental studies in understanding mechanisms of formation and removal of food deposits, aiming to find potential mitigation methods toward reduced fouling in food processing (b) Physical approaches for cleaning and disinfection in food processing environment, aiming to develop optimal management of clean-in-place process to minimize water and chemicals consumption (c) Applications of electro-membrane process for biomass valorization, including fractionation of bioactive peptides fish byproducts and removal of acetic acid from corn stover hydrolysate Dr Corvalan group's research, in collaboration with Dr. Campanella's group, has led to:Fundamental research at the nanoscale Objectives: 1: Advancing the fundamental science and application of technologies to ensure food safety and improve quality of food products 1a. Utilize innovative methods to characterize food materials Temperature dependent thermal properties measurement device TPCell 1b. Develop new and improved processing technologies Mishra with Indiana stakeholders Huang, Mishra and Corvalan for improved CIP with less chemical use and improved sustainability for food production facilities 1c. Develop mathematical models to enhance understanding of, and optimize food processes Mishra with the advancement in understanding of rapid cooling through mathematical model Optimization of thermal processes with temperature dependent thermal properties 2: Develop pedagogical methodologies for improved learning of food engineering principles. 2a. 3: Develop outreach programs to disseminate best practices for enhancing food safety and quality to stakeholders. 3a. Workshop on aseptic processing and packaging 3b. Started a new yearly workshop on validation of aseptic processing and packaging
Publications
- Type:
Conference Papers and Presentations
Status:
Published
Year Published:
2017
Citation:
Mishra D.K. 2017. Use of Process Modeling and Microbiological Validation in Food Manufacturing. Presented at the Kasetsart University invited seminar to Department of Food Science and Technology. Bangkok, Thailand. Nov 6, 2017.
- Type:
Conference Papers and Presentations
Status:
Published
Year Published:
2017
Citation:
Mishra D.K. 2017. Filing considerations for low acid particulate aseptic products. Aseptipak, Itasca, Illinois, June 20-21 2017.
- Type:
Conference Papers and Presentations
Status:
Published
Year Published:
2017
Citation:
Mishra D.K. 2017. Importance of a Product Development Course. IFT, Las Vegas, June 25-28 2017.
- Type:
Journal Articles
Status:
Published
Year Published:
2017
Citation:
Mishra, D.K., Dolan, K.D., Beck, J.V., Ozadali, F. 2017. Use of scaled sensitivity coefficient relations for intrinsic verification of numerical codes and parameter estimation for heat conduction. J. Verification, Validation, and Uncertainty Quantification. (2) 031005: 1-7.
- Type:
Journal Articles
Status:
Published
Year Published:
2017
Citation:
Muramatsu, Y., Greiby, I., Mishra, D.K., Dolan, K.D. 2017. Rapid inverse method to measure thermal diffusivity of low-moisture foods. J. Food Sci. 82(2): 420-428.
- Type:
Journal Articles
Status:
Published
Year Published:
2017
Citation:
Spotti, M., Tarhan, O., Schaffter, S., Corvalan, C. and Campanella, O. 2017, Whey Protein Gelation Induced by Enzymatic Hydrolysis and Heat Treatment: Comparison of Creep and Recovery Behavior. Food Hydrocolloids 63: 696-704.
- Type:
Journal Articles
Status:
Published
Year Published:
2017
Citation:
Suwal, S., Ketnawa, S., Liceaga, A.M.*, Huang, J.-Y.* (2017). Electro-membrane fractionation of antioxidant peptides from protein hydrolysates of rainbow trout (Oncorhynchus mykiss) byproducts. Innovative Food Science and Emerging Technologies, 45, 122-131.
- Type:
Journal Articles
Status:
Under Review
Year Published:
2017
Citation:
Suwal, S., Li, J., Engelberth, A.S., Huang, J.-Y.* Application of electro-membrane separation for recovery of acetic acid in lignocellulosic bioethanol production. Food and Bioproducts Processing. (under review)
- Type:
Journal Articles
Status:
Under Review
Year Published:
2017
Citation:
Suwal, S., Coronel-Aguilera, C.P., Auer, J., Applegate, B., Garner, A.L., Huang, J.-Y.* Mechanism characterization of bacterial inactivation of atmospheric air plasma gas and activated water using bioluminescence technology. Innovative Food Science and Emerging Technologies. (under review)
- Type:
Conference Papers and Presentations
Status:
Published
Year Published:
2017
Citation:
Mishra D.K., Dolan K.D., Beck J. V., Ozadali F. 2017. Kinetics of ascorbic acid degradation in aseptic and conventional thermal processing of sweet potato puree. Shelf Life International Meeting (SLIM). Bangkok, Thailand. Nov 1-3, 2017.
- Type:
Conference Papers and Presentations
Status:
Published
Year Published:
2017
Citation:
Benyathiar P., Selke S., Auras R., Harte B., Mishra D.K. 2017. Effect of irradiation sterilization on polylactic acid film during storage. Shelf Life International Meeting (SLIM). Bangkok, Thailand. Nov 1-3, 2017.
- Type:
Conference Papers and Presentations
Status:
Published
Year Published:
2017
Citation:
Beck JV., Mishra DK, Dolan KD. 2017. Utilization of Generalized Transient Heat Conduction Solutions in Parameter Estimation. Inverse Problems Symposium (IPS).
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Progress 10/01/15 to 09/30/16
Outputs Target Audience:Food processors in need of kinetic parametrs and thermal parameters to establish processing parameters. Changes/Problems:Dharmendra Mishra joined project on 9/28/2016 What opportunities for training and professional development has the project provided?
Nothing Reported
How have the results been disseminated to communities of interest?
Nothing Reported
What do you plan to do during the next reporting period to accomplish the goals?
Nothing Reported
Impacts What was accomplished under these goals?
Dr Corvalan group's research, in collaboration with Dr. Campanella's group, has led to:Fundamental research at the nanoscale leadingto: (a) lower cost, more effective nanosensors for rapid DNA, RNA and protein sequencing [1], (b) novel nano and micro-rheology techniques to ensure high-quality foods for consumers [2], and (c) techniques to ensure physically stable, high-quality micro-emulsions [3]. Applied research leading to new insights on whey proteingelationinduced by hydrolysis and heat treatments toensure high-quality foods for consumers and protect food processors from losses [4, 5].
Publications
- Type:
Journal Articles
Status:
Published
Year Published:
2016
Citation:
Cattani, F., Dolan, K., Oliveira, S., Mishra, D., Ferreira, C., Periago, P., Aznar, A., Fernandez, P., Valdramidis, V., (2016). One-step global parameter estimation of kinetic inactivation parameters for Bacillus sporothermodurans spores under static and dynamic thermal processes. Food Research International 89, 614-619.
- Type:
Journal Articles
Status:
Published
Year Published:
2016
Citation:
Mishra, D.K., Dolan, K.D., Beck, J.V., Ozadali, F. 2016. A novel instrument for rapid measurement of temperature-dependent thermal properties of conduction-heated food up to 140� C. J. Food Eng. 191, 19-27.
- Type:
Journal Articles
Status:
Published
Year Published:
2015
Citation:
Lu, J., Yu, J. and Corvalan, C.M., 2016. Universal Scaling Law for the Collapse of Viscous Nanopores. Langmuir, 31(31), 8618-8622.
- Type:
Journal Articles
Status:
Published
Year Published:
2016
Citation:
Lu, J., Corvalan, C.M., (2016). Soft food microrheology. Current Opinion in Food Science 9, 112-116.
- Type:
Journal Articles
Status:
Accepted
Year Published:
2016
Citation:
Lu, J., Fang, S., Corvalan, C.M., (2016). Coalescence dynamics of viscous conical drops. Physical Review E 93(2), 023111.
- Type:
Journal Articles
Status:
Published
Year Published:
2016
Citation:
Spotti, M.J., Tarhan, �., Schaffter, S., Corvalan, C., Campanella, O.H., (2017). Whey protein gelation induced by enzymatic hydrolysis and heat treatment: Comparison of creep and recovery behavior. Food Hydrocolloids 63, 696-704.
- Type:
Journal Articles
Status:
Published
Year Published:
2016
Citation:
Tarhan, O., Spotti, M.J., Schaffter, S., Corvalan, C.M., Campanella, O.H., (2016). Rheological and structural characterization of whey protein gelation induced by enzymatic hydrolysis. Food Hydrocolloids 61, 211-220.
- Type:
Conference Papers and Presentations
Status:
Published
Year Published:
2016
Citation:
Samsudin, H., Auras, R., Dolan, K.D., Mishra, D. 2015. Assessing the kinetics of a migration study by estimating a two or three-parameter models. Inverse Problems Symposium, East Lansing.
- Type:
Conference Papers and Presentations
Status:
Accepted
Year Published:
2016
Citation:
Samsudin, H., Auras, R., Dolan, K. D., Mishra, D. 2015. Assessing the kinetics of a migration study by estimating a two or three-parameter models. Inverse Problems Symposium, East Lansing, MI
- Type:
Conference Papers and Presentations
Status:
Published
Year Published:
2016
Citation:
Dolan*, K.D., Mishra, D.K., Valdramidis, V. 2016. Predictive modeling under dynamic conditions in food processing environments. European Society for Modelling and Simulation, Ghent, Belgium.
- Type:
Conference Papers and Presentations
Status:
Published
Year Published:
2016
Citation:
Dolan, K.D., Habtegebriel, H., Valdramidis, V., Mishra, D.K. 2015. Thermal processing and kinetic modeling of inactivation. In: Modeling Food Processing Operations (eds: S. Bakalis, K. Knoerzer, P. J. Fryer), pp. 37-66. Woodhead Publishing Series in Food Science, Cambridge, UK
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