Source: Applied Food Technologies, Inc submitted to
DEFINITIVE MOLECULAR MARKERS FOR SPECIATION OF FRESH AND CANNED TUNA: GENUS THUNNUS
Sponsoring Institution
National Institute of Food and Agriculture
Project Status
TERMINATED
Funding Source
Reporting Frequency
Annual
Accession No.
0230174
Grant No.
2012-33610-19967
Project No.
FLAW-2012-02159
Proposal No.
2012-02159
Multistate No.
(N/A)
Program Code
8.5
Project Start Date
Sep 1, 2012
Project End Date
Aug 31, 2015
Grant Year
2012
Project Director
Applewhite, L.
Recipient Organization
Applied Food Technologies, Inc
12085 Research Drive
Alachua,FL 32615
Performing Department
(N/A)
Non Technical Summary
Ranked as one of the world's most valuable commercial seafood, tuna species belonging to the Thunnus genus are considered the most important and endangered fish in worldwide trade. Extensive research to develop methods to distinguish Thunnus at the species level has significantly contributed to the enormous databanks of genetic information on these fish. However to date, no single approach has been successful in completely discriminating all the Thunnus species. Applied Food Technologies (AFT) has been successful in the development of molecular diagnostics for fish species identification. Our two most common approaches include PCR multiplexing utilizing species specific primers and DNA barcoding based on the COI gene sequence alignments. However as others, we have shown that neither approach is specific enough to distinguish these closely related species. A number of other methods based on RFLPs, RAPDs, SSCPs or AFLPs as well as sequencing with numerous different gene targets have also not been successful in distinguishing all species in the Thunnus genus. In Phase I of this project we targeted a different gene sequence to the COI gene that can be utilized to distinguish the six most popular Thunnus species in the fresh form and designed and tested primers that are unique to three of the six species. Success achieved in Phase I feasibility study has positioned AFT, in Phase II, to focus research and development efforts on final optimization of molecular diagnostic methods developed in Phase I and integrate additional commercially important species that are sold under the "tuna" label. Once optimized for fresh/frozen tuna, we will investigate modifications in DNA extraction protocols to enable the use of the diagnostic to identify tuna species in further processed tuna products (canned and in pouches). Our overarching goal is to deliver a commercialized multiplex diagnostic test that will readily distinguish the eight major, high-valued tuna species in commerce from one another as well as from the commonly substituted species found in commerce. The global potential of this research will serve more broadly as a template for the regulatory management of other species with close evolutionary relatedness that are also found subject to fraudulent labeling practice by providing regulators and the industry with a powerful set of tools enabling species identification and authentication. To date, regulators monitoring product labels in commerce and fisheries management groups do not have an available tool to distinguish all Thunnus species. The diagnostic developed as part of this USDA SBIR will be commercially available in our current species identification testing service as well as for use in Federal, State, public and private laboratories. This work also has potential to serve as platform technology in developing DNA-based methods for distinguishing other genetically close related species.
Animal Health Component
(N/A)
Research Effort Categories
Basic
(N/A)
Applied
100%
Developmental
(N/A)
Classification

Knowledge Area (KA)Subject of Investigation (SOI)Field of Science (FOS)Percent
50150101060100%
Goals / Objectives
The long-term goal of this project is to develop a reproducible, cost-effective molecular diagnostic that will unambiguously identify and distinguish the major commercially traded tuna species, fresh frozen and canned. While ongoing programs at AFT as well as efforts in several academic and regulatory groups continue to extend our capabilities to speciate many commercially important fish, the genetic complexity and relatedness of the major tuna species has presented significant challenges in developing a definitive diagnostic for fish of the Thunnus genus. The technical objectives of this project are to procure and authenticate reference specimens representing the additional tuna and tuna substitute species; complete design and testing of species specific primers for differentiating all genetic-related tuna species and their common substitute; test primer/probe tuna species specific strategy on real time PCR platforms; and optimize an extraction protocol for canned tuna and test with newly designed primers and probes. The final objective is to validate the lead DNA-based species identification method for both fresh/frozen and canned tuna products. The current FDA recommended protocol for DNA-based fish species identification is COI DNA barcoding, which does not differentiate all tuna species from one another. Successful development and implementation of the deliverable to be produced in this proposed project will provide a species authentication tool of significant value to seafood distributors, processors, and Federal and state regulatory agencies that is currently not available for tuna. This model system has the potential to serve as the platform technology for developing testing for other groups of closely related fish species not readily discriminated by current methods but also for other markets in the food industry dealing with issues of fraudulent labeling, traceability, species substitution as well as stock assessment and species conservation.
Project Methods
Most critical in designing accurate and defensible species identification diagnostics for tuna is to authenticate and professionally validate reference material. Working with our industry collaborators and Federal and State agencies, additional fish species to complete our current validated tuna species collection will be procured and taxonomically identified. A series of species specific primers targeting mitochondrial genes for discriminating between the six Thunnus species were designed and tested in Phase I. For the additional tuna and related species added in Phase II, comparable species specific primers will be designed and alternate gene targets will be used if necessary for ensuring discrimination among all the targeted fish species. Primer specificity for intended target will be confirmed on real time PCR platform and performance of all primers will be optimized. The universal primer set for a species-specific probe strategy designed and tested in Phase I, will be tested on the additional tuna and related species template to be included in this project. Primer/probe combinations for all tunas will initially be tested in singleplex real time PCR before converting and optimizing reactions to a multiplex format. We anticipate 3 multiplex reactions will definitively differentiate all eight highly related tunas as well as a commonly substituted species in trade. Species identification of canned and highly processed tuna remains challenging due to compromised quality of its DNA. The DNA from canned tuna will be isolated utilizing commercially available extraction kits to identify the optimal protocol that yields DNA template of quality and quantity sufficient for reproducible downstream amplification. Efforts will be made to design the most streamlined protocol that is compatible with efficient, cost-effective screening for canned tuna samples. Reproducibility of our DNA diagnostic platforms must be rigorously challenged to establish the robust nature of these methods for use in our in-house tuna species authentication test and in outside laboratory tests. We will standardize all components and methodology of the lead tuna species I.D. diagnostic to ensure reproducible results. Following proper sourcing of authenticated tuna species, we will conduct double-blind studies for ensuring accuracy of the diagnostic. We recognize the inherent variability of PCR platforms and thus will run the test for consistency using several real time PCR thermocyclers, from various manufactures with the procedure being executed by a number of technical personnel from different laboratories. Finally, independent and certified labs will conduct third party validation of the diagnostic procedures.

Progress 09/01/12 to 08/31/15

Outputs
Target Audience:The domestic seafood industry and regulators are our target audience. Once the molecular diagnostic is developed and validated, these groups will use this assay to verify tuna species in commerce. Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided?Opportunities for training and professional development are currently being provided to the seafood industry and regulators. In addition, we are using these new diagnostics in our species identification service. How have the results been disseminated to communities of interest?The results of this research have been disseminated to the seafood industry and are of great interest to the major tuna processors who now have a way to validate the products they receive and distribute. What do you plan to do during the next reporting period to accomplish the goals? Nothing Reported

Impacts
What was accomplished under these goals? Procure and authenticate reference specimens representing the additional tuna and tuna substitute species. Progress to Date: This objective was completed successfully. Complete design and testing of species specific primers for differentiating all genetic-related tuna species and their common substitute. Progress to Date: This objective has been completed successfully. Test primer/probe tuna species specific strategy on real time PCR platforms. Progress to Date: This objective has been completed successfully for the primers/probes developed for fresh/frozen tuna samples. Primers were also designed and validated for canned tuna products. Optimize an extraction protocol for canned tuna and test with newly designed primers and probes. Progress to Date: We optimized a number of steps in the DNA extraction procedure to obtain reproducible, high yield gDNA products that can be sequenced or used for conventional or real-time PCR analyses. Validate the lead DNA-based species identification method for fresh/frozen and canned tuna products. Progress to Date: This objective has been completed successfully.

Publications


    Progress 09/01/13 to 08/31/14

    Outputs
    Target Audience: The domestic seafood industry and regulators are our target audience. Once the molecular diagnostic is developed and validated, these groups will use this assay to verify tuna species in commerce. Changes/Problems: We have encountered problems with the reproducibility of our DNA extraction method for canned tuna products. We are investigating the inconsistencies and trying to optimize the extraction. What opportunities for training and professional development has the project provided? Opportunities for training and professional development will be provided to the seafood industry and regulators once the objectives of the grant are accomplished. How have the results been disseminated to communities of interest? Dissemination of the results to communities of interest are in progress. What do you plan to do during the next reporting period to accomplish the goals? In the no-cost extension period we will optimize the DNA extaction of canned tuna products, test the primers and probes that have been developed, and validate the DNA based species identification method for canned tuna.

    Impacts
    What was accomplished under these goals? The Technical Objectives for this project are stated below. For clarity, the progress to date is stated within each technical objective. In the first year, Technical Objective 1 was completed. During this period, Objective 2 was completed and Objectives 3 and 5 were completed with fresh/frozen tuna products. We obtained a no-cost extension to complete Objective 4 and then complete Objective 3 and 5 for canned tuna products. 1. Procure and authenticate reference specimens representing the additional tuna and tuna substitute species. Progress to Date: This objective has been completed successfully. 2. Complete design and testing of species specific primers for differentiating all genetic-related tuna species and their common substitute. Progress to Date: This objective has been completed successfully. 3. Test primer/probe tuna species specific strategy on real time PCR platforms. Progress to Date: This objective has been completed successfully for the primers/probes developed for fresh/frozen tuna samples. Primer/probe development is on-going for canned tuna products. 4. Optimize an extraction protocol for canned tuna and test with newly designed primers and probes. Progress to Date: We requested a no-cost extension on this project to complete this objective. We are optimizing a number of steps in the DNA extraction procedure in order to obtain high enough yields of PCR product and better sequence data. 5. Validate the lead DNA-based species identification method for fresh/frozen and canned tuna products. Progress to Date: This objective has been completed successfully for the primers/probes developed for fresh/frozen tuna samples. The diagnostic for canned tuna products will be developed as soon as Obj. 4 is completed.

    Publications


      Progress 09/01/12 to 08/31/13

      Outputs
      Target Audience: The domestic seafood industry and regulators are our target audience. Once the molecular diagnostic is developed and validated, these groups will use this assay to verify tuna species in commerce. Changes/Problems: The work on this project is progressing as planned. All expenditures to date have been as proposed. We have not encountered any problems and expect to successfully complete the project as scheduled. What opportunities for training and professional development has the project provided? Opportunities for training and professional development will be provided to the seafood industry and regulators once the objectives of the grant are accomplished. How have the results been disseminated to communities of interest? Dissemination of the results to communities of interest are in progress. What do you plan to do during the next reporting period to accomplish the goals? Technical Objectives 2-5 will be completed in year two. We are continuing to optimize the DNA extraction procedure using canned tuna samples and will then test both short and longer amplicon primers using our optimized method using both fresh and canned tuna. 3. Test primer/probe tuna species specific strategy on real time PCR platforms. The universal primer set for a species-specific probe strategy designed and tested in Phase I, will be tested on the additional tuna and related species template to be included in this project. Primer/probe combinations for all tunas will initially be tested in singleplex real time PCR before converting and optimizing reactions to a multiplex format. We anticipate 3 multiplex reactions will definitively differentiate all 8 highly related tunas as well as a commonly substituted species in trade. 5. Validate the lead DNA-based species identification method for fresh/frozen and canned tuna products. Reproducibility of our DNA diagnostic platforms must be rigorously challenged to establish the robust nature of these methods for use in our in-house tuna species authentication test and in outside laboratory tests. We will standardize all components and methodology of the lead tuna species I.D. diagnostic to ensure reproducible results. We will conduct double-blind studies for ensuring accuracy of the diagnostic. We recognize the inherent variability of PCR platforms and thus will run the test for consistency using several real time PCR thermocyclers, from various manufactures with the procedure being executed by a number of technical personnel from different laboratories. Finally, independent and certified labs will conduct third party validation of the diagnostic procedures. Progress to Date: This technical objective will be initiated after the other objectives are complete.

      Impacts
      What was accomplished under these goals? The Technical Objectives for this project are stated below. For clarity, the progress to date is stated within each technical objective. In the first year, Technical Objective 1 was completed; and significant progress made with Technical Objectives 2 and 4. Objective 3 will be completed in the first few months of year two and Objective 5 will be initiated after the other objectives are complete. Procure and authenticate reference specimens representing the additional tuna and tuna substitute species. Most critical in designing accurate and defensible species identification diagnostics for tuna is to authenticate and professionally validate reference material. Working with our industry collaborators and Federal and State agencies, additional fish species to complete our current validated tuna species collection have been procured and taxonomically identified. Progress to Date: This objective has been completed successfully. We are currently working with all of the tuna below for this project. 2. Complete design and testing of species specific primers for differentiating all genetic-related tuna species and their common substitute. A series of species specific primers targeting mitochondrial genes for discriminating between the six Thunnus species were designed and tested in Phase I. For the additional tuna and related species added in Phase II, comparable species specific primers will be designed and alternate gene targets will be used if necessary for ensuring discrimination among all the targeted fish species. Primer specificity for intended target will be confirmed on real time PCR platform and performance of all primers will be optimized. Progress to Date: We have made significant progress on this objective. We are conducting a two pronged approach to meet this objective: (1) design primers that amplify a ~450 bp amplicon of the mtDNA CR gene and (2) design primers that amplify shorter (~100 bps) segments of this gene. The rationale for this two pronged approach is that we currently get more consistent PCR amplification results from canned tuna samples using primers that yield shorter amplicons (<100 bp). This objective will be completed early in year two. 4. Optimize an extraction protocol for canned tuna and test with newly designed primers and probes. Species identification of canned and highly processed tuna remains challenging due to the compromised quality of its DNA. The DNA from canned tuna will be isolated utilizing commercially available extraction kits to identify the optimal protocol that yields DNA template of quality and quantity sufficient for reproducible downstream amplification. Efforts will be made to design the most streamlined protocol that is compatible with efficient, cost-effective screening for canned tuna samples. Progress to Date: We have worked closely with our collaborators to make significant progress with this objective. We have optimized a number of procedures in our DNA extraction protocol in order to obtain higher quality PCR products of 450 bps in length from canned tuna samples that can be sequenced. We are currently optimizing a number of steps in the DNA extraction procedure in order to obtain even higher yields of PCR product and better sequence data.

      Publications