Source: UNIV OF HAWAII submitted to NRP
DEVELOPMENT OF COMBINED CONTINUOUS FLOW MICROWAVE AND PULSED OHMIC HEATING TECHNOLOGIES FOR RAPID AND UNIFORM HEATING OF MULTIPHASE FOODS
Sponsoring Institution
National Institute of Food and Agriculture
Project Status
COMPLETE
Funding Source
Reporting Frequency
Annual
Accession No.
0219594
Grant No.
2009-65503-05786
Cumulative Award Amt.
(N/A)
Proposal No.
2009-02351
Multistate No.
(N/A)
Project Start Date
Sep 1, 2009
Project End Date
Aug 31, 2013
Grant Year
2009
Program Code
[93430]- Improving Food Quality and Value
Recipient Organization
UNIV OF HAWAII
3190 MAILE WAY
HONOLULU,HI 96822
Performing Department
Human Nutrition, Food & Animal Sciences
Non Technical Summary
The key objectives of this Research Strengthening Standard Grant proposal are (1) to design a continuous flow microwave and ohmic combination heater for particulate foods and (2) to test for its heating uniformity and food qualities in terms of sensory values and lethal sterility. Uniform heating of particulate foods (i.e. soups containing vegetables and meats) has been a challenge because temperatures of solid cores could lag behind that of liquid. Non-uniform heat treatment of particulate foods would allow for inadequate microbial destruction and therefore, the full recovery of foodborne pathogens, in turn threatening the public health. Instant and volumetric heating of microwave and ohmic technologies are outstanding for food quality preservation; however, microwaves can lead to partial over-heating and cold spots, whereas ohmic heating requires additional blanching pretreatment of a product to obtain desired electrical conductivities for heating uniformity. To eliminate individual technology limitations, it is proposed to combine both microwave and ohmic heating technologies in such that solid particles with lower electrical conductivities will be heated via microwaves with strong penetration depth, and a carrier medium with higher salt concentrations will be treated by ohmic current. As the first attempt to design a microwave and ohmic combination heater in a continuous mode, this approach will effectively address one of the program FY 2009 Priorities, 2. Generating the knowledge base for advanced and innovative processing, engineering, and technologies that enhance food quality attributes and development and application of analytical characterization techniques of physical, chemical, biological, and sensory natures.
Animal Health Component
30%
Research Effort Categories
Basic
30%
Applied
30%
Developmental
40%
Classification

Knowledge Area (KA)Subject of Investigation (SOI)Field of Science (FOS)Percent
50150102020100%
Knowledge Area
501 - New and Improved Food Processing Technologies;

Subject Of Investigation
5010 - Food;

Field Of Science
2020 - Engineering;
Goals / Objectives
The goal of this project is to test the microwave and ohmic combination heating technology for heating uniformity of particulate foods. Combining two heating technologies to eliminate the downsides would be beneficial for uniform heating of multiphase foods since it can allow liquid parts of the product to be heated immediately via current and solid particles, independent of their conductivity values, can be heated to the cores very rapidly via microwave. Specific research objectives addressed in this project are as follows: Objective A: Design a continuous flow microwave and ohmic combination heater. Objective B: Explore the heating patterns of solid-liquid mixtures in a combined heater. The project director (PD)'s lab is equipped with a 5kW custom-designed dual magnetrons microwave heater and a 2kW pulsed ohmic heater. The proposed combination of independent two units will include a series of helical coil heat exchangers and non-conductive ohmic chamber with impedance matching and circuit design as needed. Temperature values of solid particles (i.e. carrot, potato, and meat cubes) and liquid carrier medium via the influence of microwave and ohmic frequencies will be measured and analyzed. Objective C: Measure dielectric properties and electrical conductivities of solid-liquid mixtures. Objective D: Develop the flow and heat transfer model for combined microwave and ohmic heating system. Maxwell's equations governing the electromagnetic field distribution will be solved using the finite element method (FEM) based commercial code. The solution will be coupled with the flow and thermal modules to solve the momentum and heat equations using the computational fluid dynamics (CFD) codes. Objective E: Calculate and compare the efficiency of energy conversion for combined two heating technologies. Microwave heating which is alone poor energy efficient will be complemented by the use of ohmic technology since the energy transfer efficiency of ohmic process is close to 100%. Objective F: Estimate metal ions migration and fouling occurrence in foods under the ohmic treatment. Concentration of Fe and Cr migrated into the heating media taken as measures of electrode corrosion will be estimated using inductively coupled plasma - mass spectrometer (ICP-MS). Fouling mass in a dry form after treatment will be collected by rubbing off and weighed from the electrode. The expected outputs are: 1. Uniform heat distribution for multiphase foods will be obtained by the proposed technology. 2. Microwave and ohmic combination heating patterns of particulate foods will be predictable using numerical modeling based on computational fluid dynamics (CFD). 3. Combined short-term volumetric heating will effectively minimize undesired electrochemical reactions at the electrode interfaces. 4. Combined two technologies will increase the overall energy efficiency by 20%. 5. Combined two technologies will enhance food qualities, compared to the control. 6. The project outcomes found in laboratory are highly likely to find their applications on a massive scale in numerous segments of food and the US industry.
Project Methods
Objective A: Design a continuous flow microwave and ohmic combination heater. Microwave cavities that will be modified from the existing unit in the PD's lab will be combined with an ohmic chamber where solid-liquid mixture will flow under the influence of external electric field strength between the two electrodes. The diameters of coil typed heat exchangers will be determined based on the sizes of particles entering into the unit. Impedance matching between the microwave power source and loaded cavity needs to be carried out to minimize wave reflection. Objective B: Explore the heating patterns of solid-liquid mixtures in a combined heater Temperature values of solid particles (i.e. carrots, potatoes, and meats) and liquid medium via microwave with pulse width modulation (PWM), and ohmic frequencies will be measured and analyzed. Carrot, potato, and beef cubes will cut to approximately 1.5 cm each side. Each sample will be stored in a refrigerator prior to use in the experiments. The PD proposes that 2% NaCl solution and 1% carboxymethylcellulose (CMC) solution with 2% NaCl could be good candidates as carrier media. Objective C: Measure dielectric properties and electrical conductivities of solid-liquid mixtures. Dielectric properties of the solid particles and carrier medium will be measured using an open-ended coaxial probe (Model Agilent 85070E, Agilent Technologies) connected to a network analyzer. Electrical conductivities of solid particles and carrier fluid will be calculated from the resistance of samples and the geometry of the ohmic cell. Objective D: Develop the flow and heat transfer model for combined microwave and ohmic heating system. The flow pattern of multiphase foods in a combined microwave and ohmic heating unit can be solved by means of a general purpose CFD code, i.e. Fluent (Fluent, Lebanon, NH) that is based on the finite volume method (FVM). We also need separate commercial code, COMSOL (COMSOL, Inc., Burlington, MA) to get the power density term as a function of time. The approach used in coupling microwaves with heat transfer is to solve Maxwell equations inside a microwave cavity (COMSOL) and then couple the solution with the thermodynamic and hydrodynamic modules to solve for temperature and flow patterns of solid-liquid mixtures (Fluent) Objective E: Calculate and compare the efficiency of energy conversion for combined two heating technologies. Input power to run for (1) microwave, (2) ohmic and (3) combined microwave and ohmic heating units will be separately measured using a wattmeter. The energy conversion efficiency will be calculated based on the amount of energy accumulated in solid particles and carrier medium. Objective F: Estimate metal ions migration and fouling occurrence in foods under the ohmic treatment. Concentration of Fe and Cr migrated into the heating media taken as measures of electrode corrosion will be estimated using inductively coupled plasma - mass spectrometer (ICP-MS, available in Agricultural Diagnostic Service Center, University of Hawaii).

Progress 09/01/09 to 08/31/13

Outputs
Target Audience: Nothing Reported Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided? Nothing Reported How have the results been disseminated to communities of interest? Nothing Reported What do you plan to do during the next reporting period to accomplish the goals? Nothing Reported

Impacts
What was accomplished under these goals? 1. Novel dual cylindrical microwave chambers equipped with an ohmic heating tube were designed and fabricated to maximize the electric field strength for uniform heat treatment of particulate foods. Designing of the combination chamber was optimized and validated using the numerical simulation for electric field and potential distributions. Thermal profiles of solid-liquid mixtures consisting of sodium chloride solution (0.5 ~ 2% concentration), chicken, and potato particulates at different mass fractions (10 and 15%) were collected and compared for individual and combination heating modes when the exit temperature of either solid or liquid phase reached approximately 80°C in 36 sec. Results indicated that particle size (0.5 and 1 cm in length) and salt concentration substantially affected temperature variations between solution and particulates in ohmic heating. On the other hand, for microwave heating the solution temperature always lagged behind the particle temperature with salt concentrations up to 1.25%, regardless of particle size and mass fraction; however, an opposite pattern was observed in the food mixtures including 2% salt concentration. The maximum temperature differences between solid and liquid phases obtained by individual microwave and ohmic heating were 7.1 ± 1.7 and 11.9 ± 2.9 °C, respectively; while the combination heating exhibited no significant temperature gaps (maximum temperature difference < 3.08°C) at low salt concentrations (up to 1.25%). The controllable ranges of key variables to permit heating uniformity in the developed heater were obtained using the factorial analysis and response optimzer. 2. A numerical model using COMSOL codes was developed to validate uniform heating of particulate foods in a continuous flow microwave (MW) and ohmic (OH) combination heating chamber. The developed model was integrated with microwave heating, ohmic heating, incompressible laminar flow, forced-coupling method (FCM), heat transfer and arbitrary Langrangian-Eulerian (ALE) moving mesh technique. The solid particles were simulated to experience hydrodynamic viscous drag and pressure forces resulting from motion relative to the fluid. The stress tensors of forces exerted on the surfaces of the particles were successfully formulated by use of the FCM module. The large deformation and movement of geometric mish containing trajectories of particles inside the feeding tube were successfully executed in the state of the transient mode. The outlet temperatures of particulate foods under microwave, ohmic and combination heating also were in a good agreement with experimental data within the error of 4%.

Publications

  • Type: Journal Articles Status: Published Year Published: 2013 Citation: Abdullah, S., Lee, S.H., Cho, I., Choi, W., and Jun, S. 2013. Pasteurization of Kava Juice using Novel Continuous Flow Microwave Heating Technique. Food Science and Biotechnology 22(4): 961-966
  • Type: Journal Articles Status: Under Review Year Published: 2013 Citation: Lee, S.H., Choi, W., Yoon, S.K., and Jun, S. 2013. Development of a dual cylindrical microwave and ohmic combination heater for minimization of thermal lags in the processing of particulate foods. Innovative Food Science and Emerging Technologies
  • Type: Journal Articles Status: Submitted Year Published: 2013 Citation: Choi, W., Lee, S.H., and Jun, S. 2013. Numerical Approach of a Continuous Flow Microwave and Ohmic Heating for Particulate Foods using a Finite Element Method. Transactions of the ASABE
  • Type: Journal Articles Status: Published Year Published: 2013 Citation: Nguyen, L.T., Choi W., Lee, S.H., Jun, S. 2013. Exploring the Heating Patterns of Multiphase Foods in a Continuous Flow, Simultaneous Microwave and Ohmic Combination Heater. Journal of Food Engineering 116(1): 65-71
  • Type: Journal Articles Status: Submitted Year Published: 2013 Citation: Lee, S.H. and Jun, S. 2013. Current and Emerging Combination Technologies for Food Processing: A Review. Food and Bioprocess Technology
  • Type: Conference Papers and Presentations Status: Published Year Published: 2013 Citation: Jun, S. 2013. Continuous Flow, Simultaneous Microwave and Ohmic Combination Heating Technology for Multiphase Foods. The 2013 IFT Annual Meeting, July 14-16, Chicago, IL (268-04)
  • Type: Conference Papers and Presentations Status: Published Year Published: 2013 Citation: Lee, S.H., Choi, W., and Jun, S. 2013. Continuous Flow, Simultaneous Microwave, and Ohmic Combination Heating Technology for Multiphase foods: Simulation for Thermal Uniformity and Lethal Effectiveness. The 2013 IFT Annual Meeting, July 14-16, Chicago, IL (031-21)
  • Type: Conference Papers and Presentations Status: Published Year Published: 2013 Citation: Choi, W., Lee, S.H., and Jun, S. 2013. Application of an ohmic thawing unit combined with a microwave heater. The 2013 IFT Annual Meeting, July 14-16, Chicago, IL (031-18)
  • Type: Journal Articles Status: Submitted Year Published: 2013 Citation: Abdullah, S., Choi, W., and Jun, S. 2013. Mathematical Modeling and Numerical Simulation for Predictive Retention of Antioxidant Activity of Grape Juice Pasteurized with Continuous Flow Ohmic Heating. International Journal of Agricultural and Biological Engineering


Progress 09/01/11 to 08/31/12

Outputs
OUTPUTS: The design of the combination heater was optimized by non-destructive numerical analysis. Teflon tube with a pair of ring-shaped electrodes housed inside both ends was installed at the middle of dual cylindrical microwave cavities. The combination heater was evaluated using food mixtures consisting of potato and chicken cubes (about 1 cm^3), and carboxymethylcellulose (CMC) solution. The maximum temperature differences found in solid-liquid mixture under individual microwave and ohmic heating were approximately 8.1 and 8.0 degC, respectively. Temperature difference exists even between various solid particles during ohmic heating rather than microwave heating. However, when microwave and ohmic heating was simultaneously applied, there was little significant temperature difference between solid particles and liquid phases (less than 2 degC). The energy efficiency of ohmic and microwave heating were 94.2 and 55.4%, respectively. However, the hybrid combination heating increased energy conversion efficiency by 24.7% as compared to microwave heating. Two papers have been accepted and three talks were given at the conference meetings at Japan and Chicago, IL. Nguyen, L.T., Choi W., Lee, S.H., Jun, S. 2012. Exploring Heating Patterns of Multiphase Foods in a Continuous Flow, Simultaneous Microwave and Ohmic Combination Heater. Journal of Food Engineering (Accepted) Abdullah, S., Lee, S.H., Cho, I., Choi, W., and Jun, S. 2012. Pasteurization of Kava Juice using Novel Continuous Flow Microwave Heating Technique. Food Science and Biotechnology (Accepted) Nguyen, L.T.,Choi, W., Lee, S.H. and Jun, S. 2012. Exploring the Heating Patterns of Multiphase Foods using Continuous Flow, Simultaneous Microwave and Ohmic Combination Heating Technique. FOOMA JAPAN 2012: International Food Machinery and Technology Exhibition. Abdullah, S., Choi, W., and Jun, S. 2012. Simulation of Antioxidants Activity of Grape Juice with Continuous Flow Ohmic Heating, The 2012 IFT Annual Meeting, June 26-28, Las Vegas, NV (077-01) Lee, S.H., Choi, W., Nguyen, L., and Jun, S. 2012. Continuous Flow, Simultaneous Microwave, and Ohmic Combination Heating Technology for Thermal Uniformity of Multiphase Foods, The 2012 IFT Annual Meeting, June 26-28, Las Vegas, NV (077-16) PARTICIPANTS: Nothing significant to report during this reporting period. TARGET AUDIENCES: Food beverage companies to heat process meat vegetable soups and chunky mixed fruit juice. PROJECT MODIFICATIONS: Not relevant to this project.

Impacts
The findings will open new and very promising opportunities to thermally process particulate foods (i.e. meat vegetable soup and chunky mixed fruit juice) with improved uniformity, organoleptic, nutritional quality and reduced food safety problems.

Publications

  • No publications reported this period


Progress 09/01/10 to 08/31/11

Outputs
OUTPUTS: Based on the preliminary data obtained from the experiment conducted at the first year of this project, a continuous flow, simultaneous microwave and ohmic combination heater was designed and fabricated. The project in Year 2 was intended to explore and compare the heating patterns of particle-liquid mixtures under individual heating (microwave and ohmic heating) and the combination heating. A pair of ring-shaped electrodes made of titanium was inserted into both ends of Teflon pipe for ohmic heating and the pipe was vertically installed at the center of microwave cavity for simultaneous microwave and ohmic combination heating. Prior to the temperature measurement of the particle-liquid mixture (carrot cubes and carboxymethylcellulose (CMC) solution) treated using the combination heating technology, the electric field and temperature distribution of the food mixture inside the cavity were simulated using a commercial finite element methods (FEM) software (COMSOL 3.4, COMSOL, Inc., Palo Alto, CA). Single heat treatments showed opposite results; carrot particles were heated faster than CMC solution by 8.1 degC under microwave heating and however, CMC solution was heated up faster than solid particles by 8 degC when ohmic current was applied. Uniform heating was achieved under simultaneous combination heating and the temperature difference between particles and CMC solution was only 0.5 degC. The experimental data was in good agreement with simulation data. Hybrid combination heating also increased the energy efficiency by 10.6%, as compared to microwave heating. Power control of both heating methods and combination logic in terms of the frequency and wave characteristics will be intensively researched in the next phase of this project. PARTICIPANTS: Nothing significant to report during this reporting period. TARGET AUDIENCES: Nothing significant to report during this reporting period. PROJECT MODIFICATIONS: Nothing significant to report during this reporting period.

Impacts
The result from this study clearly showed that uniform heating pattern of solid-liquid food mixtures is achievable in a continuous mode when the combination heating technology was applied. This is critical because under-processed solid particles are always at risk in terms of food safety. The pretreatment process such as salt infusion can be removed from the line once the developed technology is accepted for commercial food processing. Combined ohmic and microwave heating technology can significantly contribute to energy savings. This technology will compensate for the safety level of the microbial lethality in particulate food products and will be effectively applied for sterilization processing of low acid multiphase foods containing large particulates as well.

Publications

  • Lee, S.H., Nguyen, L.T., Choi, W., & Jun, S. (2011). Exploring the heating patterns of multiphase foods in a continuous flow, simultaneous microwave and ohmic combination heater. The 23rd Annual CTAHR Students Symposium, Honolulu, HI.
  • Jun, S. (2011). Exploring the heating patterns of multiphase foods in a continuous flow, simultaneous microwave and ohmic combination heater. ICEF Annual Meeting, Athens, Greece.
  • Nguyen, L.T., Choi, W., Lee, S.H., Jun, S. (2011). Exploring the heating patterns of multiphase foods in a continuous flow, simultaneous microwave, and ohmic combination heater. IFT Annual Meeting & Food Expo, New Orleans, LA.
  • Choi, W., Nguyen, L.T., Lee, S.H., and Jun, S. (2011). A microwave and ohmic combination heater for uniform heating of a liquid-particle food mixture. Journal of Food Science,76, E576 - E585
  • 61/488,107, Continuous flow microwave and ohmic combination heating technique for multiphase foods. Provisional patent application filed on May 19, 2011.


Progress 09/01/09 to 08/31/10

Outputs
OUTPUTS: In the first year of the project, the concept of combined heating techniques was explored in a small scale experimental setup including a static test cell. Before a continuous flow microwave and ohmic combination heater can be made, a simple, custom made static heater could be helpful to gain insights into the heating patterns of the liquid-particle mixtures. Simple food models composed of vegetable particulates (1cm cubes) and sodium chloride solution were used in the study. The viscosity of liquid sample was adjusted using carboxymethylcellulose (CMC) so the particulates can be suspended in the solution. This property is important as the particulates will be pumped through the continuous flow heater in the next phase of the study. To better understand the heating uniformity of the multiphase mixtures, temperature distribution was investigated by numerical simulation with the aid of a commercial FEM software (COMSOL 3.4, COMSOL, Inc., Palo Alto, CA) and was validated with experimental data. Extensive data of electrical and dielectric properties of foods as a function of temperature were also experimentally determined. Under studied conditions, experimental data showed that liquid temperature was uniform during ohmic heating as compared to microwave heating. However, for a continuous flow heater, the mixing of liquid will enhance the temperature uniformity and only the average liquid temperature is critical in this case. Solid particle, after 2 min of microwave heating, was heated faster than liquid about 13.0 degree Celsius. For ohmic heating, liquid was heated faster than solid and the thermal gradient was about 21.0 degree Celsius. When two heating modes were combined, temperature of solid particles ended up close to that of the liquid, leading to a more uniform temperature throughout the product. The obtained simulation results showed similar trends and had a good agreement with experimental data. Works under progress included design and fabrication of the continuous flow, sequential microwave and ohmic combination heater. The developed device will help confirm the concept in the continuous flow mode that is more realistic for practical applications. The heater development involved design, optimization of energy conversion and electric field distribution. Simulation for continuous flow combination heating had been conducted and still under progress. The results will be reported in the next phase of the study. PARTICIPANTS: Dr. Loc Nguyen Junior Researcher Department of Human Nutrition, Food and Animal Sciences University of Hawai`i at Manoa 1955 East-West Road Honolulu, HI 96822-2321 Tel: + 808 -956-6588 e-mail: loc749@hawaii.edu TARGET AUDIENCES: Food industries: Development of a continuous flow microwave and ohmic combination heater would provide a new insight for food sterilization in food industries. Continuous flow processes of particulate foods are hampered by FDA concerns over the residence time distributions. If a product containing food particulates can be heated rapidly and uniformly, a significant quality improvement may be expected and the process of FDA approval should be easier. PROJECT MODIFICATIONS: Not relevant to this project.

Impacts
The findings during the initial stage of this study clearly demonstrated that a product containing food particulates can be heated rapidly and uniformly by combined microwave and ohmic heating. Liquid was heated faster by ohmic current and solids were heated by microwave, independent of their electrical conductivity. Unlike conventional thermal processing, ohmic or mircrowave heating, the combined heating eliminates the downsides of the individual heating technologies. Given this data, we believe that the development of a microwave and ohmic combination heater could provide new options for food sterilization and provides a promising opportunity to improve both the safety and quality of processed foods.

Publications

  • Nguyen, L.T., Choi, W., Lee, S.H., Jun, S. Exploring the Uniformity in Thermal Patterns of Multiphase Foods Using the Novel Microwave and Ohmic Combination Heating Technology. 2010 IFT Annual Meeting, Chicago, IL.