Source: SUMMIT SEED, INC. submitted to
UTILIZE EXTRACTED DDGS (INVIVE) FOR WEED CONTROL AND ENHANCED PLANT GROWTH IN HORTICULTURAL APPLICATIONS.
Sponsoring Institution
National Institute of Food and Agriculture
Project Status
COMPLETE
Funding Source
Reporting Frequency
Annual
Accession No.
0213560
Grant No.
2008-33610-18996
Cumulative Award Amt.
(N/A)
Proposal No.
2008-00199
Multistate No.
(N/A)
Project Start Date
Jun 15, 2008
Project End Date
Feb 14, 2009
Grant Year
2008
Program Code
[8.8]- Biofuels and Biobased Products
Recipient Organization
SUMMIT SEED, INC.
3676 W 9000 N ROAD
MANTENO,IL 60950-3340
Performing Department
(N/A)
Non Technical Summary
Ethanol production is a rapidly growing industry in the United States where corn is the principal feedstock. Dried distiller grains (DDGs) are a co-product of the dry milling process, which currently accounts for approximately 75 percent of the domestic ethanol production. The production of DDGs in the U.S. was 7.3 million tons in 2004 and is expected to increase to over 16 million tons by 2012. DDGs are currently used almost exclusively as animal feed, therefore, finding alternative uses for DDGs, with greater profit potential are needed as DDGs supply increases. The problem is the DDGs contain an estimated 10% fatty oils that causes the byproduct to go rancid if not used in a relatively short time period. The opportunity is to utilize the by-product from the DDGs which could become a new standard in our horticultural industry for organic weed control and enhanced plant growth with an organic product. This organic based product has the added benefit of being plant based to avoid all the problems associated with manure based products. And, with sky rocketing fertilizer prices make this organic product more cost effective everyday just based on its fertilizer value. The potential for this product is very broad in a market that is hungry for organic based products. And the organic demand is increasing from the home gardener to golf courses to organic farming.
Animal Health Component
100%
Research Effort Categories
Basic
(N/A)
Applied
100%
Developmental
(N/A)
Classification

Knowledge Area (KA)Subject of Investigation (SOI)Field of Science (FOS)Percent
2132300115050%
5111510100050%
Goals / Objectives
Our objective is to utilize Extracted DDGs (Dried Distillers Grains) for weed control and enhanced plant growth in horticultural applications. The goal of our Phase 1 is to first extract an estimated 10 percent oil from the DDGs to be sold off to reduce our cost in the DDGs while reducing a dependency on foreign oil and then to prove that Extracted DDGs can be a cost effective way to increase weed control and enhance plant growth in horticultural applications. Initial research demonstrates that Extracted DDGs was more effective than the DDGs in that they showed improved weed control, has higher nitrogen content, making the product a stable product for storage, and eliminated offensive odors associated with DDGs after applications on the ground. The anticipated results are to turn a potentially burdensome supply of low value DDGs into a valuable resource by utilizing the product, what we are calling Invive, in an organic herbicide, fertilizer and soil amendment product that we would expect to use in the horticultural industry. Invive has the potential to reduce our demand on synthetic fertilizer such as Urea Nitrogen that uses natural gas during the production process. Furthermore, we expect to prove that Invive will reduce our need to use synthetic herbicides for weed control, all while producing better results than conventional methods.
Project Methods
Initial research has demonstrates that by removing the oils the extracted DDGs were more effective than the DDGs in that they showed improved weed control, has higher nitrogen content, makes the product a stable product for storage and eliminated offensive odors associated with DDGs after applications on the ground. Un-extracted DDGs contain approximately 10 percent oil by weight. We will be using two methods for removing or reducing the oil content of the DDGs. The first is using conventionally organic solvents such as hexane are used to extract oils from plant material such as soybeans which be used for feasibility. The second method will be a degermed DDGs which is a new process whereby the corn germ is removed prior to the corn being processed for ethanol production. The germ of corn contains most of the oil content. This process will produce low oil (estimated 3.5 percent) content DDGs that may prevent the product from becoming rancid and still possess the organic weed control and positive growth traits that the extruded DDGs have demonstrated. To determine the pre-emergence weed control bare ground by applying un-extracted DDGs, Extracted DDGs and Degermed both as surface applied preemergence applications and incorporated into the soil additives. A field site with a natural population of weeds will be used. A broadleaf herbicide will be applied this fall to control existing broadleaf weeds. Each treatment will be surface applied with a separate set of bare ground treatments with the products incorporated to a depth of 4 cm. The experiment will be replicated four times and visually rated for individual broadleaf and grass weed species that are present Ratings will be conducted 0.5, 1, and 2 months after treatment. There will be 14 treatments and the trials will be initiated in April to coincide with standard industry practice. We will also determine the turf quality, length of nitrogen response, growth, and weed control effects on 10 Kentucky Bluegrass varieties by applying both un-extracted DDGs, Extracted DDGs, Degermed DDGs, Urea Nitrogen and Nutralene (synthetic, slow-release nitrogen carrier) as topical applications to measure turf quality and length of response of treatments applied at 2 and 4 pounds actual nitrogen per 1,000 square feet at Summit Seed Turfgrass Center. Each treatment will be replicated three times across Kentucky bluegrass varieties planted in 4-foot strips. The treatments will be applied 4 feet strips across the Kentucky bluegrass varieties yielding 4 foot by 4 foot square blocks. Digital ratings of turfgrass quality will be collected at 2, 4, 6, 8, 10, and 12 weeks after application. Summit Seed personnel will be using a relatively new digital rating system developed by Dr. Kenneth Hignight of Advanta Seed West, Albany, Oregon. The system enables us to make non bias precision ratings for the turfgrass plot evaluations. We believe this will offer us more creditability to conduct research at our turfgrass center.

Progress 06/15/08 to 02/14/09

Outputs
OUTPUTS: To date the DDGS extraction process at the ARS-USDA NCUAR Lab has been contacted with ethanol alone. In summary, objective 1.0 is seeing progress where Summit Seed is characterizing the chemical components of the hexane extract and developing methods for separating these components. In doing this they will develop methods for separation of extract into product streams. Additional fractionation samples were received after our field testing was completed. Objective 2.0 started August 11th, 2008, where Summit Seed determined the pre-emergence weed control bare ground by applying un-extracted DDGS, extracted DDGS, and degermed fractionated corn both as surface applied pre-emergence applications and incorporated into the soil additives. These experiments were held in the field in 5' by 5' plots at Summit Seed Turfgrass Center located in the back of the building. The first set of digital ratings of the weed control plots were conducted 2.5 weeks after application on September 1st, 2008. A field site with a natural population of weeds was used. A broadleaf herbicide was applied fall 2008 to control existing broadleaf weeds. The experiment was replicated three times and visually rated for individual broadleaf and grass weed species that are present. There were 14 treatments and the trials were initiated in April to coincide with standard industry practice. All of the treatments used in Objective 3.0 were tested by CLC Labs to determine accurate nitrogen content prior to treatment initiation. Dr. Charles Darrah, President of CLC Labs recommended the experiment to determine length of response and turf quality from each product. Each treatment was replicated three times across Kentucky bluegrass varieties planted in 4-foot strips. The treatments were applied in 4' strips across the Kentucky bluegrass varieties yielding 4' by 4' square blocks. Digital ratings of turfgrass quality were collected at 2, 4, 6, 8, and 10 weeks after application. Summit Seed personnel used a relatively new digital rating system developed by Dr. Kenneth Hignight of Advanta Seed West, Albany, Oregon. The system enables us to make non bias precision ratings for the turfgrass and bedding plant evaluations. We believe this will offer us more creditability to conduct research at our turfgrass center. Summit Seed instructed Dr. Hank Wilkinson from the University of Illinois to carry out objective 4.0 where he measured the increase or decrease in water infiltration by adding the Invive product to the soil profile. Wilkinson used a 6 inch diameter PVC tube. These materials were layered onto the top of a field soil. The topsoil was 10 inches deep and the layer of materials was one-half inch deep. The soil and the materials were dry when layered. Each material was tested individually and compared against the field soil. Additionally, 200 ml of water was poured onto the top of each test soil and the following measurements were made: 1. Depth of water penetration after 1.0 min (dry infiltration rate) 2. Time for water to penetrate 10 inches (saturated flow rate). PARTICIPANTS: Project Director: Ed Lee was responsible for over-all coordination of research at Summit Seed, Inc. and coordination of the consulting company working on the project. Co - Project Director: Ron Edwards assisted in the over-all coordination of research at Summit Seed, Inc. and coordination of the consulting company working on the project. Authorized Organization Representative: Shad Taylor was responsible for preparing proper documentation to be reported and recorded during the Phase I efforts. Digital ratings were conducted by Shad Taylor with the assistance of Ed Lee out in the field research plots. Project Consultant: Steve Vaughn was assisted by an undergraduate student along side the consulting services of Steve F. Vaughn. Both assisted in the initial research of the Invive product. Project Consultant: Jerry Hatfield of the USDA Soil Tilth Lab was the center for utilizing state of the art growth chambers where the temperature, light, and relative humidity on the soil was controlled. Evaluations of Invive were conducted here to measure the microbial activity. Project Consultant: Bruce Branham helped act as a consultant for this project overseeing/reviewing our research plan and statistically helped rank the plot ratings. Project Contractor: Roger Mohr of Viobin, U.S.A. extracted the oils to produce Invive. TARGET AUDIENCES: Nothing significant to report during this reporting period. PROJECT MODIFICATIONS: Nothing significant to report during this reporting period.

Impacts
Summit Seed, Inc. has found that the advantage to using the liquid CO2 over just ethanol is that we may be able to selectively extract the oil without any contaminating polar compounds and by adding ethanol to the liquid CO2 we can get out the other compounds. Research at the NCAUR is centered on developing cost-effective methods and environmentally-friendly extraction and isolation of the oil. Product streams will consist of the Invive and Purrfect Sense Cat Litter where continued testing in the horticultural applications and cat litter markets will be conducted by Summit Seed, Inc. Unfortunately, during the Phase I research period, objective 2.0 resulted in negative response with Invive being applied as a topical application with no real noticeable control on weeds including the industry standard Corn Gluten Meal. This will lead us to better research the product as a soil additive component. The results during the first few weeks influenced our decisions to not follow through with the surface applications and to disregard taking any digital rating results for ground cover control. Research conducted at Summit Seed even with the irrigation in place at least gave us incite into the characteristics and capabilities of the DDGS product as just a topical applicant. During Phase II efforts we plan to better research the product as a powder solution and a mixed in soil solution. Additionally, during the Phase I research period Dr. Vaughn experimented with the extracted DDGS as a cat litter solution. With the removal of the oils the granular material becomes very porous allowing for an increased capacity as an absorbent material. Initial research has shown that the extracted DDGS material could be used as a cat litter product having the ability to absorb liquid/solid waste. Dr. Vaughn has promising additives that eliminate the odors. There will be opportunities to further introduce the extracted DDGS material into the absorbent spill cleanup market. During Objective 3.0 the Invive product displayed competitiveness with the quick release Urea Nitrogen fertilizer and other synthetic fertilizers. Results early on showed substantial support in our initial trials during Phase I that Invive is ranking in the top listings for digital quality including factors such as percent cover, density, and color. When walking out on the plots observers can see the distinct difference in quality with the different fertilizer applications. Objective 4.0 results were neutral in that Invive neither increases nor decreases the water infiltration levels by adding to the soil profile. Lastly, Objective 5.0 proved to be more difficult to measure during the Phase I research period. After talking the task over with Dr. Wilkinson and Dr. Hatfield they advised per personal communication that the microbial activity is hard to measure and the results are inconsistent, and would be better to look at better vegetation and better turf results during the on going research into the Phase II period. A Phase II grant has been submitted for further evaluations of the Invive product and Purrfect Sense cat litter.

Publications

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