Source: UNIVERSITY OF ILLINOIS submitted to
UNSATURATED FLUID TRANSPORT MECHANISMS IN POROUS FOOD BIOPOLYMERS
Sponsoring Institution
National Institute of Food and Agriculture
Project Status
NEW
Funding Source
Reporting Frequency
Annual
Accession No.
1014188
Grant No.
(N/A)
Project No.
ILLU-698-308
Proposal No.
(N/A)
Multistate No.
(N/A)
Program Code
(N/A)
Project Start Date
Oct 3, 2017
Project End Date
Sep 30, 2022
Grant Year
(N/A)
Project Director
Takhar, PA, SI.
Recipient Organization
UNIVERSITY OF ILLINOIS
2001 S. Lincoln Ave.
URBANA,IL 61801
Performing Department
Food Science & Human Nutrition
Non Technical Summary
Numerous food science applications involve transport of fluids in the unsaturated porous biopolymeric matrices. An unsaturated matrix contains gas (air-vapor mixture), which may flow due to pressure or concentration gradients in the biopolymeric matrix. Examples of unsaturated fluid transport applications in food science include frying of foods involving flow of water vapors to oil, water loss, and oil uptake; expansion of biopolymers exiting a high pressure extruder due to water flash off followed by bubble growth; drying of foods with fissures or at low moisture contents; and microwave heating of foods. The gas phase complicates the underlying physical mechanisms because it is compressible and can leak from the porous channels, resulting in fluid-gas interphases which further cause capillary forces in the system. There is little fundamental work addressing unsaturated transport in food science applications although there is an abundance of processes involving fluid flow of this type. To improve the quality of foods and efficiency of food processes involving unsaturated fluid transport, the proposed research will utilize unsaturated transport theory developed for biopolymers using the framework of Hybrid Mixture Theory (HMT). The project will involve solution of the developed equations such as generalized Darcy's law, capillary pressure relations, and the multiscale mass balance equation for frying and drying of foods. Experiments will be conducted to measure the material parameters and obtain validation data.
Animal Health Component
0%
Research Effort Categories
Basic
70%
Applied
30%
Developmental
(N/A)
Classification

Knowledge Area (KA)Subject of Investigation (SOI)Field of Science (FOS)Percent
5015010202050%
5025010202050%
Goals / Objectives
The long-term goal is to describe unsaturated transport mechanisms for food science applications and solve the modeling equations to improve the quality of foods and efficiency of processes. The specific objectives are:1. To describe the unsaturated fluid transport mechanisms using a system of hybrid mixture theory based modeling equations.2. To solve the modeling equations for calculating various quality parameters for processes such as frying and drying of foods.3. To validate the model predictions by making comparisons to the experimental data.
Project Methods
Solution of the Hybrid Mixture Theory based equations such as generalized Darcy's law, capillary pressure relations, and the multiscale mass balance equation will be obtained for the unsaturated transport processes such as frying and drying of foods. The finite element method will be used to solve the equations for the moving geometry of a food. The solution will involve transforming the equations from Eulerian to Lagrangian coordinates, performing the computations and transforming the results back to the moving coordinates. The experiments will be conducting using frying and drying equipment available in PI's laboratory. Capillary pressure, which plays an important role in unsaturated transport processes, will either be calculated using water activity data for foods or using surface tension measured with a contact angle meter.

Progress 10/01/19 to 09/30/20

Outputs
Target Audience:Members of the food science and engineering research community and food industry professionals. Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided?The project partially supported two graduate students and one undergraduate student, who received training on mathematical modeling using the multiscale equations, solving the equations using the finite element method, conducting the microwave frying experiments, and analysis of quality attributes of foods. How have the results been disseminated to communities of interest?The results were disseminated by making conference presentations atthe Conference of Food Engineers and American Institute of Chemical Engineers conference focused on food materials. These conferences are attended by both the academic research community and food industry professionals. What do you plan to do during the next reporting period to accomplish the goals?Additional frying experiments are planned in the current year. The graduate students working on the project will continue to receive training on mathematical modeling and experimental analysis on frying of foods. The effect frying parameters such as temperature, duration and microwave poweron transport of fluids and species will be investigated. One student will work on the modeling aspects and the second student will work on the experimental aspects of frying. Both students will compare their results to developcomplementary information for making the fried products healtheir for consumers.

Impacts
What was accomplished under these goals? The hybrid mixture theory-based multiscale model for predicting ice formation in foods during freeze-thaw cycles was solved using the finite element method. The model can explain the fluid, species, heat transport, ice formation, thermomechanical changes, and the freezing point depression inside the foods during freezing. Volume changes during freezing were calculated using the stresses due to pore pressure and the phase-change based mechanical strain. The model predictions were validated by making comparisons to the experimental data. The model could predict freezing point depressions in foods due to solute migration to unfrozen regions with greater accuracy than a commonly used empirical equation published in the freezing literature. The amplitude, frequency and duration of the freeze-thaw cycles causing ice formation, melting and growth that could damage the food microstructure were investigated. The effect of opening and closing of freezer doors by consumers on ice formation in the food matrix was studied. The conditions causing less damage to the food structure were identified. The frozen food industry can utilize the results of this research to improve the design and operation of their freezers. The frying mechanisms were studied by conducting conventional and microwave-frying experiments. The aim of these experiments was to test the hypothesis that the changes in pore pressure inside the food matrices is the primary driver of oil uptake. The pore pressure becomes negative during frying. For the frying experiments, Russet potatoes were cut into cylindrical shapes. They were blanched in boiling water for twominutes and immediately cooled to room temperature in cold water. Each batch of blanched potatoes was fried at two temperatures for different times using the conventional frying method or with conventional combined with microwaves. The moisture content values were measured for the blanched and fried fries. The fat content was measured by extracting it using the Soxhlet method. For the same amount of moisture loss, microwave frying resulted in lower fat uptake than conventional frying. This was expected to have occurred due to an increase in the pore pressure due to additional energy imparted by the microwaves to the water molecules. In addition, the effect of post frying sample handling on the surface oil removal was studied by comparing the gravity method with the surface oil absorption method. Drainage of the surface oil via gravity method led to its lower reduction than by patting the samples with paper towels. Additional experiments are scheduled to be conducted this year.

Publications

  • Type: Journal Articles Status: Submitted Year Published: 2021 Citation: Zhao, Y., Kumar, P.K., Sablani, S. and Takhar, P.S. 2021. Two-scale Unsaturated Transport of Fluids, Species and Heat in Biopolymers During Freezing. American Institute of Chemical Engineers Journal, AICheJ (Submitted).


Progress 10/01/18 to 09/30/19

Outputs
Target Audience:Members of the target audience included the food science and engineering research communitiesand food industry professionals. Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided?The project partially supported two graduate students and one undergraduate student, who received training on mathematical modeling using multiscale equations, solving the equations using the finite element method, and conducting the fluid transport experiments. How have the results been disseminated to communities of interest?The results were disseminated by making conference presentations at Institute of Food TechnologistsAnnual Meeting and the Conference of Food Engineers. These conferences are attended by both the academic research community and byfood industry professionals. What do you plan to do during the next reporting period to accomplish the goals?Additional experiments on frying and drying of foods will be conducted. New students will continue to receive training on experimental and mathematical modeling aspects of fluid transport in foods. Manuscripts currently under preparation will be submitted for publication.

Impacts
What was accomplished under these goals? Hybrid mixture theory-based equations were utilized for describing transport mechanisms during drying and freezing of foods. The equations were solved for predicting ice formation in frozen foods, and quality changes and nutritional attributes during drying. Experiments on frying of foods were conducted to elucidate unsaturated transport mechanisms. Foodmoisture content and oil content were measured to determine parameters causing fewer stress cracks.

Publications


    Progress 10/03/17 to 09/30/18

    Outputs
    Target Audience:Two research presentations were made at the Conference of Food Engineers in 2018 to the research community, students and food industry professionals. Examples on unsaturated transport in food systems were given in these presentations. Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided?Project trained an undergraduate and a graduate student on unsaturated transport mechanisms in food systems. How have the results been disseminated to communities of interest? The results were disseminated by making presentationsat the Conference of Food Engineers annual meeting. What do you plan to do during the next reporting period to accomplish the goals?Additional experimental work on microwave heating of foods will be conducted. Due to variability during frying, experimental trials with overten replications per treatment will be conducted. Moisture sorption/desorption related experimental and modeling work will also be conducted to study the effect of glass transition on quality changes in foods.

    Impacts
    What was accomplished under these goals? Since the project started this year, the plan was setup and students were trained. Experimental work on unstaturated transport during microwave frying of foods was conducted by an undergraduate student. Comparison of conventional frying and microwave frying pressure profiles inside french fries were made. Additional experiments are planned for the current year. A graduate student was trained to model moisture sorption in foods undergoing glass-transition. Moisture sorption model is expected to be completed in current year.

    Publications