Source: TDA RESEARCH, INC. submitted to
A NEW RENEWABLE POLYMER FROM BIO OIL
Sponsoring Institution
National Institute of Food and Agriculture
Project Status
COMPLETE
Funding Source
Reporting Frequency
Annual
Accession No.
0233798
Grant No.
2013-33610-20834
Cumulative Award Amt.
$100,000.00
Proposal No.
2013-00181
Multistate No.
(N/A)
Project Start Date
Jul 1, 2013
Project End Date
Feb 28, 2014
Grant Year
2013
Program Code
[8.8]- Biofuels and Biobased Products
Recipient Organization
TDA RESEARCH, INC.
12345 WEST 52ND AVENUE
WHEAT RIDGE,CO 80033
Performing Department
(N/A)
Non Technical Summary
This project will develop a catalytic process to manufacture a new renewable and degradable bio-plastic that could be used to replace polyethylene in many applications, including those that constitute a large part of land and ocean litter such as bags, food packaging and disposable tableware.
Animal Health Component
100%
Research Effort Categories
Basic
(N/A)
Applied
100%
Developmental
(N/A)
Classification

Knowledge Area (KA)Subject of Investigation (SOI)Field of Science (FOS)Percent
51174102000100%
Goals / Objectives
In this Phase I project TDA Research, Inc. (TDA) will develop an economically viable process for producing a novel, 100% renewable high performance thermoplastic from cellulosic feedstocks. This polymer is made by polymerization of a non-toxic monomer that can be obtained in large quantities as a co-product of a commercial thermochemical process that is used to convert forest products to diesel. In preliminary work TDA proved that our renewable monomer can be polymerized to make a high molecular weight product having good stability, high stereo-regular structure, and mechanical properties that are intermediate between those of low density polyethylene (LDPE) and high density polyethylene (HDPE). Unfortunately, the synthetic method used to prove feasibility is currently too expensive for making a product that will have to compete with commodity petrochemical thermoplastics. Thus, the objective of this project is to develop a cheaper and scalable alternative production process. TDAs technology offers disruptive advantages over competitive bio-plastics because the production of the monomer does not compete with the food supply chain (as with corn-derived materials), the polymer is biodegradable, easily compostable and the monomer and degradation products are non-toxic and non-persistent chemicals. Disposable tableware and food packaging are our early target applications. Furthermore, this technology promises a sustainable economic advantage due to its synergy with bio-diesel production, which reduces capital investment.
Project Methods
In preliminary work TDA Research Inc. demonstrated that our renewable monomer can be polymerized to make a high molecular weight product having good stability, high stereo-regular structure, and mechanical properties that are similar to those of polyethylene. Unfortunately, the synthetic method used to prove feasibility is currently too expensive to compete with commodity petrochemical thermoplastics. Thus, the objective of this project is to develop a scalable alternative production process. The material produced will be characterized to determine its chemical structure, thermo-mechanical, barrier and degradation properties. The properties of the material made with the new polymerization methods will be compared to those of the product made by the current method to determine whether it is the same or a different stereo-isomer form. We will then conduct a cost and engineering analysis of the monomer scale-up and polymer production.

Progress 07/01/13 to 02/28/14

Outputs
Target Audience: companies that produce monomers by fast pyrolysis and companies that produce biopolymers by polymerization of renewable monomers Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided? Nothing Reported How have the results been disseminated to communities of interest? Results will be presented at the ACS NAtional Meeting in August of 2013 in San Francisco What do you plan to do during the next reporting period to accomplish the goals? Nothing Reported

Impacts
What was accomplished under these goals? During this Phase I project TDA successfully devised a catalytic method for the synthesis of a novel, 100% renewable high performance thermoplastic from cellulosic feedstocks. The novel process is environmentally friendly since it uses mild conditions, a non-toxic catalyst, and a stable and recyclablereaction medium. With this development it has become apparent that that novel renewable polymer represents a disruptive technology within the renewable polymer market arena because: the monomer can be obtained in high purity from agricultural feedstocks. Its production can be integrated with the production of bio-diesel and does not compete with the food supply chain; the polymer is biodegradable and compostable and the degradation products have a benign environemetal profile; the polymer can be produced via a green process that is economical and scalable.

Publications

  • Type: Conference Papers and Presentations Status: Accepted Year Published: 2014 Citation: oral presentation has been scheduled for the technical program of the 248th ACS National Meeting that will be held in San Francisco, California, August 10-14, 2014. PAPER ID: 19198 PAPER TITLE: Novel renewable thermoplastic from the fast pyrolysis of cellulosic feedstock (final paper number: 684) DIVISION: POLY: Division of Polymer Chemistry SESSION: Green Polymer Chemistry: Biobased Materials and Biocatalysis SESSION START TIME: August 13, 2014, 1:30 pm August 13, 2014 from 4:25 pm to 4:45 pm