Source: NORTH DAKOTA STATE UNIV submitted to
PROCUREMENT OF A ZETASIZER FOR NANOMATERIAL CHARACTERIZATION TO UNDERSTAND FOOD SAFETY ISSUES RELATED TO NANOPARTICLE-FOOD INTERACTIONS
Sponsoring Institution
National Institute of Food and Agriculture
Project Status
TERMINATED
Funding Source
Reporting Frequency
Annual
Accession No.
1005554
Grant No.
2015-67018-23107
Project No.
ND05440
Proposal No.
2014-05684
Multistate No.
(N/A)
Program Code
A1331
Project Start Date
Feb 15, 2015
Project End Date
Feb 14, 2016
Grant Year
2015
Project Director
Bezbaruah, A. N.
Recipient Organization
NORTH DAKOTA STATE UNIV
(N/A)
FARGO,ND 58105
Performing Department
Civil and Environmental Engineering
Non Technical Summary
Nanoparticles (<100 nm) are finding increasing use in consumer products, electronics, structural materials, pollution control, and medicine. There has been a huge effort to understand the benefits and adverse effects of nanotechnology on the agriculture and food sectors. There are more than 150 nanotechnology-based food products in the market already and a number of nanotechnology-based products for agricultural application (including fertilizers) are expected. The nanoparticles that find their way to agriculture are typically dispersed in aqueous media (irrigated water or pore water). The science involved in dispersion will be better understood with additional information on zeta potential of the nanoparticles. The zeta potential is known to be pH dependent and it is known that pH changes in the rhizosphere (plant root zone) in a dynamic way depending on what is introduced to that zone, and the resulting changes in zeta potential are expected to influence the stability and reactivity of the particles. Further, nanoparticles are functionalized to perform specific tasks and functionalization changes their properties. The measurement of zeta potential of the nanomaterials becomes even more important at this stage as the zeta potential will also determine how they behave with food, associated microorganisms, and molecular level materials. The zeta potential of particles may also change in the presence of natural organic matters (NOM) and clays and that will be important to understand to elucidate plant/food-nanoparticle interactions. The interactions of nanoparticles also depend on the particle size, and the particle size changes depending where the particles are present (for example, under dry or wet conditions). The goal the present project is to procure a Zetasizer (equipment) that can measure zeta potential and diameter of nanoparticles. It can also measure the flow behavior of some nanomaterials. With the Zetasizer on campus, the Project Director and other researchers will be able get much faster and accurate measurements of the nanoparticle properties and conduct studies involving the nanomaterials and fresh crop at macro and molecular levels. The procurement of a Zetasizer will impact food safety research presently conducted by the PD and his collaborators. The PDs will be also able explore new areas of research once equipped with the Zetasizer. The equipment will help in analytical capacity building as a number of post-graduate, graduate and undergraduate students will be trained to use it and they will be able to use it for their research. The equipment will also be used by other researchers at North Dakota State University and outside and they will be benefitted from the state-of-the-art equipment.
Animal Health Component
0%
Research Effort Categories
Basic
100%
Applied
(N/A)
Developmental
(N/A)
Classification

Knowledge Area (KA)Subject of Investigation (SOI)Field of Science (FOS)Percent
1027410202050%
1330210107050%
Goals / Objectives
Project Goals: Immediate goal of this project is to procure a Zetasizer for the measurement of (1) particle size with specific interest on nanoparticles, (2) zeta potential, and (3) molecular weight of biological particles and use these measurements in research pertaining to nanoparticle and food crop interactions. Long-term Goals: The long-term and overarching goal of this project is to enhance the research capability of the Project Director (PD) and the faculty involved in area of food safety. The PD and faculty involved in this proposal are working on areas related food safety and agriculture. The PD and other faculty members will be using this equipment to characterize nano- and microparticles (including bacteria and fungi) in aqueous media and interpret and use the results to improve agriculture practices in the United States with specific emphasis of agricultural food. The team put together by the PD are multi-disciplinary in nature and will be a perfect group to work on complex problems related to immerging technologies (e.g., nanotechnology). Establishing long-term collaborations will help the PD to achieve the overarching goal in this project. The PD and other participating faculty plan to continue their collaborations so that they can contribute to the body of knowledge in nanotechnology through life-cycle studies, and help in developing models for sustainable nanotechnology products for food and agricultural applications. Specific Objectives: The specific objective of this research is to procure the equipment and set it up for immediate use by the PD and other major users' research groups
Project Methods
Efforts: The Zetasizer will be procured as soon possible. The manufacturer/supplier will install the instrument and arrage for a training program.Evaluation: The PD will keep track of instrument hours used by researchers and collect information whether the results will be published in the near future. The PD will also monitor the number of peer reviewed papers published with data generated by this new instrument.

Progress 02/15/15 to 02/14/16

Outputs
Target Audience:University faculty, researchers, graduate, and undergraduate students within North Dakota State University. Changes/Problems: Nothing Reported What opportunities for training and professional development has the project provided?The PD, 3 graduate researchers, and 2 undergraduate researchers were trained on how to use this piece equipment. More researchers have shown interest to be trained such that they can use it for their research. How have the results been disseminated to communities of interest?The PD communicated to other researchers about the availablity of the equipment on campus. Research publications based on data generated using the new instrument have not been published yetbut are expected soon. What do you plan to do during the next reporting period to accomplish the goals?This is the final report. The project is completed.

Impacts
What was accomplished under these goals? The instrument has been used to characterize nanomaterials in different environmental conditions. The PD has done some preliminary work on wheat flour and how the particle size changes on hydration of the flour. This is new equipment and the PD is expecting to use it more and more in the near future. The mail goal of procuring the equipment and making it available for the PD's research group and others on campus has been accomplished.

Publications